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Spectra for:
Mitsuyasu Ushijima, Noriko Komoto, Yoshimi Sugizono, Ikuko Mizuno, Masanori Sumihiro, Makoto Ichikawa, Minoru Hayama, Nobuo Kawahara, Takahisa Nakane, Osamu Shirota, Setsuko Sekita, Masanori Kuroyanagi

Compound 1 B PROSAPOGENIN;3-O-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID

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PROSAPOGENIN;3-O-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID
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13C NMR Spectrum

Compound 5A PROSAPOGENIN;3-O-BETA-D-GLUCOPYRANOSYL-(1->3)-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID

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PROSAPOGENIN;3-O-BETA-D-GLUCOPYRANOSYL-(1->3)-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID
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13C NMR Spectrum

#1;LANCEMASIDE-A;3-O-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID-28-O-BETA-D-XYLOPYRANOSYL-(1->3)-BETA-D-XYLOPYRANOSYL-(1->4)

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#1;LANCEMASIDE-A;3-O-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID-28-O-BETA-D-XYLOPYRANOSYL-(1->3)-BETA-D-XYLOPYRANOSYL-(1->4)
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13C NMR Spectrum

#2;LANCEMASIDE-B;3-O-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID-28-O-BETA-D-XYLOPYRANOSYL-(1->3)-BETA-D-XYLOPYRANOSYL-(1->4)

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#2;LANCEMASIDE-B;3-O-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID-28-O-BETA-D-XYLOPYRANOSYL-(1->3)-BETA-D-XYLOPYRANOSYL-(1->4)
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13C NMR Spectrum

#3;LANCEMASIDE-C;3-O-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID-28-O-BETA-D-XYLOPYRANOSYL-(1->4)-ALPHA-L-RHAMNOPYRANOSYL-(1-

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#3;LANCEMASIDE-C;3-O-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID-28-O-BETA-D-XYLOPYRANOSYL-(1->4)-ALPHA-L-RHAMNOPYRANOSYL-(1-
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13C NMR Spectrum

#4;LANCEMASIDE-D;3-O-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID-28-O-ALPHA-L-RHAMNOPYRANOSYL-(1->2)-[BETA-D-GLUCOPYRANOSYL-(

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#4;LANCEMASIDE-D;3-O-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID-28-O-ALPHA-L-RHAMNOPYRANOSYL-(1->2)-[BETA-D-GLUCOPYRANOSYL-(
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13C NMR Spectrum

#5;LANCEMASIDE-E;BETA-D-GLUCOPYRANOSYL-(1->3)-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID-28-O-BETA-D-XYLOPYRANOSYL-(1->3)-BE

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#5;LANCEMASIDE-E;BETA-D-GLUCOPYRANOSYL-(1->3)-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID-28-O-BETA-D-XYLOPYRANOSYL-(1->3)-BE
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13C NMR Spectrum

#6;LANCEMASIDE-F;3-O-BETA-D-GLUCOPYRANOSYL-(1->3)-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID-28-O-BETA-D-XYLOPYRANOSYL-(1->3

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#6;LANCEMASIDE-F;3-O-BETA-D-GLUCOPYRANOSYL-(1->3)-BETA-D-GLUCURONOPYRANOSYL-(3-BETA,16-ALPHA)-DIHYDROXY-OLEAN-12-EN-28-OIC-ACID-28-O-BETA-D-XYLOPYRANOSYL-(1->3
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13C NMR Spectrum

#7;LANCEMASIDE-G;3-O-BETA-D-GLUCURONOPYRANOSYL-(2-BETA,3-BETA,16-ALPHA)-TRIHYDROXY-OLEAN-12-EN-28-OIC-ACID-28-O-BETA-D-XYLOPYRANOSYL-(1->3)-BETA-D-XYLOPYRANOSY

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#7;LANCEMASIDE-G;3-O-BETA-D-GLUCURONOPYRANOSYL-(2-BETA,3-BETA,16-ALPHA)-TRIHYDROXY-OLEAN-12-EN-28-OIC-ACID-28-O-BETA-D-XYLOPYRANOSYL-(1->3)-BETA-D-XYLOPYRANOSY
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13C NMR Spectrum

Citation

Citation CHEM.PHARM.BULL.,56,308(2008)
Journal Chemical and Pharmaceutical Bulletin
Issue 3
Volume 56
Page(s) 308-314
Year 2008
Author(s) Mitsuyasu Ushijima, Noriko Komoto, Yoshimi Sugizono, Ikuko Mizuno, Masanori Sumihiro, Makoto Ichikawa, Minoru Hayama, Nobuo Kawahara, Takahisa Nakane, Osamu Shirota, Setsuko Sekita, Masanori Kuroyanagi
Publisher Pharmaceutical Society of Japan
DOI 10.1248/cpb.56.308