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Spectra for:
Andrew Pelter, Robert S. Ward, D. Martin Jones, Peter Maddocks

Compound 1 3A (-)-(3S,4R,6R)-3-(3',4'-DIMETHOXY-ALPHA-HYDROXYBENZYL)-4-(3'',4''-DIMETHOXYBENZYL)-BUTYROLACTONE

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(-)-(3S,4R,6R)-3-(3',4'-DIMETHOXY-ALPHA-HYDROXYBENZYL)-4-(3'',4''-DIMETHOXYBENZYL)-BUTYROLACTONE
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13C NMR Spectrum

Compound 4A (-)-(4R,5R)-4-[3',4'-Dimethoxy-.alpha.,.alpha.-bis(phenylthio)benzyl]-5-(1-menthyloxy)butyrolactone

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(-)-(4R,5R)-4-[3',4'-Dimethoxy-.alpha.,.alpha.-bis(phenylthio)benzyl]-5-(1-menthyloxy)butyrolactone
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13C NMR Spectrum

Compound 4B (-)-(4R,5R)-4-[3',4'-Methylenedioxy-.alpha.,.alpha.-bis(phenylthio)benzyl]-5-(1-menthyloxy)butyrolactone

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(-)-(4R,5R)-4-[3',4'-Methylenedioxy-.alpha.,.alpha.-bis(phenylthio)benzyl]-5-(1-menthyloxy)butyrolactone
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13C NMR Spectrum

Compound 5A (-)-(4R,5R)-4-(3',4'-Dimethoxybenzyl)-5-(1-menthyloxy)butyrolactone

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(-)-(4R,5R)-4-(3',4'-Dimethoxybenzyl)-5-(1-menthyloxy)butyrolactone
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13C NMR Spectrum

Compound 5B (-)-(4R,5R)-4-(3',4'-Methylenedioxybenzyl)-5-(1-menthyloxy)butyrolactone

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(-)-(4R,5R)-4-(3',4'-Methylenedioxybenzyl)-5-(1-menthyloxy)butyrolactone
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13C NMR Spectrum

Compound 6A (-)-(3S,4R,5R,6R)-3-(3',4'-DIMETHOXY-ALPHA-HYDROXYBENZYL)-4-[3'',4''-DIMETHOXY-ALPHA,ALPHA-BIS-(PHENYLTHIO)-BENZYL]-5-(1-MENTHYLOXY)

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(-)-(3S,4R,5R,6R)-3-(3',4'-DIMETHOXY-ALPHA-HYDROXYBENZYL)-4-[3'',4''-DIMETHOXY-ALPHA,ALPHA-BIS-(PHENYLTHIO)-BENZYL]-5-(1-MENTHYLOXY)
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13C NMR Spectrum

Compound 6B (-)-(3S,4R,5R,6R)-3-(3',4'-METHYLENEDIOXY-ALPHA-HYDROXYBENZYL)-4-[3'',4''-DIMETHOXY-ALPHA,ALPHA-BIS-(PHENYLTHIO)-BENZYL]

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(-)-(3S,4R,5R,6R)-3-(3',4'-METHYLENEDIOXY-ALPHA-HYDROXYBENZYL)-4-[3'',4''-DIMETHOXY-ALPHA,ALPHA-BIS-(PHENYLTHIO)-BENZYL]
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13C NMR Spectrum

Compound 6C (-)-(3S,4R,5R,6R)-3-(3',4',5'-TRIMETHOXY-ALPHA-HYDROXYBENZYL)-4-[3'',4''-METHYLENEDIOXY-ALPHA,ALPHA-BIS

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(-)-(3S,4R,5R,6R)-3-(3',4',5'-TRIMETHOXY-ALPHA-HYDROXYBENZYL)-4-[3'',4''-METHYLENEDIOXY-ALPHA,ALPHA-BIS
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13C NMR Spectrum

Compound 7A (-)-(3S,4R,5R,6R,7S)-3-(3',4'-DIMETHOXY-ALPHA-HYDROXYBENZYL)-4-[3'',4''-DIMETHOXY-ALPHA-(PHENYLTHIO)-BENZYL]-5-(1-MENTHYLOXY)-BUTYROLACTONE

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(-)-(3S,4R,5R,6R,7S)-3-(3',4'-DIMETHOXY-ALPHA-HYDROXYBENZYL)-4-[3'',4''-DIMETHOXY-ALPHA-(PHENYLTHIO)-BENZYL]-5-(1-MENTHYLOXY)-BUTYROLACTONE
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13C NMR Spectrum

Compound 7B (-)-(3S,4R,5R,6R,7S)-3-(3',4'-METHYLENEDIOXY-ALPHA-HYDROXYBENZYL)-4-[3'',4''-DIMETHOXY-ALPHA-(PHENYLTHIO)-BENZYL]-5-(1-MENTHYLOXY)-BUTYROLACTONE

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(-)-(3S,4R,5R,6R,7S)-3-(3',4'-METHYLENEDIOXY-ALPHA-HYDROXYBENZYL)-4-[3'',4''-DIMETHOXY-ALPHA-(PHENYLTHIO)-BENZYL]-5-(1-MENTHYLOXY)-BUTYROLACTONE
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13C NMR Spectrum

Compound 8A (+)-(3S,4R,5R,6R,7R)-3-(3',4'-DIMETHOXY-ALPHA-HYDROXYBENZYL)-4-[3'',4''-DIMETHOXY-ALPHA-(PHENYLTHIO)-BENZYL]-5-(1-MENTHYLOXY)-BUTYROLACTONE

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(+)-(3S,4R,5R,6R,7R)-3-(3',4'-DIMETHOXY-ALPHA-HYDROXYBENZYL)-4-[3'',4''-DIMETHOXY-ALPHA-(PHENYLTHIO)-BENZYL]-5-(1-MENTHYLOXY)-BUTYROLACTONE
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13C NMR Spectrum

Compound 8B (+)-(3S,4R,5R,6R,7R)-3-(3',4'-METHYLENEDIOXY-ALPHA-HYDROXYBENZYL)-4-[3'',4''-DIMETHOXY-ALPHA-(PHENYLTHIO)-BENZYL]-5-(1-MENTHYLOXY)-BUTYROLACTONE

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(+)-(3S,4R,5R,6R,7R)-3-(3',4'-METHYLENEDIOXY-ALPHA-HYDROXYBENZYL)-4-[3'',4''-DIMETHOXY-ALPHA-(PHENYLTHIO)-BENZYL]-5-(1-MENTHYLOXY)-BUTYROLACTONE
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13C NMR Spectrum

Compound 9A (-)-(3S,4R,5R,6R)-3-(3',4'-DIMETHOXY-ALPHA-HYDROXYBENZYL)-4-(3'',4''-DIMETHOXYBENZYL)-5-(1-MENTHYLOXY)-BUTYROLACTONE

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(-)-(3S,4R,5R,6R)-3-(3',4'-DIMETHOXY-ALPHA-HYDROXYBENZYL)-4-(3'',4''-DIMETHOXYBENZYL)-5-(1-MENTHYLOXY)-BUTYROLACTONE
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13C NMR Spectrum

Compound 9B (-)-(3S,4R,5R,6R)-3-(3',4'-METHYLENEDIOXY-ALPHA-HYDROXYBENZYL)-4-(3'',4''-DIMETHOXYBENZYL)-5-(1-MENTHYLOXY)-BUTYROLACTONE

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(-)-(3S,4R,5R,6R)-3-(3',4'-METHYLENEDIOXY-ALPHA-HYDROXYBENZYL)-4-(3'',4''-DIMETHOXYBENZYL)-5-(1-MENTHYLOXY)-BUTYROLACTONE
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13C NMR Spectrum

Compound 9C (-)-(3S,4R,5R,6R)-3-(3',4',5'-TRIMETHOXY-ALPHA-HYDROXYBENZYL)-4-(3'',4''-METHYLENEDIOXYBENZYL)-5-(1-MENTHYLOXY)-BUTYROLACTONE

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(-)-(3S,4R,5R,6R)-3-(3',4',5'-TRIMETHOXY-ALPHA-HYDROXYBENZYL)-4-(3'',4''-METHYLENEDIOXYBENZYL)-5-(1-MENTHYLOXY)-BUTYROLACTONE
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13C NMR Spectrum

Compound 13B (-)-(3S,4R,6R)-3-(3',4'-METHYLENEDIOXY-ALPHA-HYDROXYBENZYL)-4-(3'',4''-DIMETHOXYBENZYL)-BUTYROLACTONE

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(-)-(3S,4R,6R)-3-(3',4'-METHYLENEDIOXY-ALPHA-HYDROXYBENZYL)-4-(3'',4''-DIMETHOXYBENZYL)-BUTYROLACTONE
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13C NMR Spectrum

Compound 13C (-)-6-EPI-PODORHIZOL

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(-)-6-EPI-PODORHIZOL
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13C NMR Spectrum

Compound 14A (-)-(1S,2R,3R)-1-[3',4'-Dimethoxyphenyl)-3-(hydroxymethyl)-6,7-dimethoxy-1,2,3,4-tetrahydronaphthalene-2-carboxylic acid lactone

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(-)-(1S,2R,3R)-1-[3',4'-Dimethoxyphenyl)-3-(hydroxymethyl)-6,7-dimethoxy-1,2,3,4-tetrahydronaphthalene-2-carboxylic acid lactone
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13C NMR Spectrum

Compound 14B (-)-(1S,2R,3R)-1-(3',4'-METHYLENEDIOXYPHENYL)-3-(HYDROXYMETHYL)-6,7-DIMETHOXY-1,2,3,4-TETRAHYDRONAPHTHALENE-2-CARBOXYLIC-ACID-LACTONE

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(-)-(1S,2R,3R)-1-(3',4'-METHYLENEDIOXYPHENYL)-3-(HYDROXYMETHYL)-6,7-DIMETHOXY-1,2,3,4-TETRAHYDRONAPHTHALENE-2-CARBOXYLIC-ACID-LACTONE
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13C NMR Spectrum

Compound 14C (-)-DEOXYISOPODOPHYLLOTOXIN

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(-)-DEOXYISOPODOPHYLLOTOXIN
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13C NMR Spectrum

Citation

Citation J.CHEM.SOC.PERKIN-1,2621(1993)
Journal Journal of the Chemical Society, Perkin Transactions 1
Issue 21
Page(s) 2621
Year 1993
Author(s) Andrew Pelter, Robert S. Ward, D. Martin Jones, Peter Maddocks
Publisher Royal Society of Chemistry (RSC)
DOI 10.1039/p19930002621