Spectra for:
Satoshi Tsuchiya, Toshiaki Sunazuka, Tomoyasu Hirose, Ryuma Mori, Toshiaki Tanaka, Masato Iwatsuki, Satoshi Ōmura
Compound I (+)-(2S,4R)-4-[4'-(TERT.-BUTYLDIMETHYLSILOXY)-BUTYL]-2-(PARA-METHOXYPHENYL)-1,3-DIOXANE
![(+)-(2S,4R)-4-[4'-(TERT.-BUTYLDIMETHYLSILOXY)-BUTYL]-2-(PARA-METHOXYPHENYL)-1,3-DIOXANE](/api/compound/He1df55qxZc.png?h=300&w=458 "(+)-(2S,4R)-4-[4'-(TERT.-BUTYLDIMETHYLSILOXY)-BUTYL]-2-(PARA-METHOXYPHENYL)-1,3-DIOXANE")
Compound IV (+)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXAN-1-OL
![(+)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXAN-1-OL](/api/compound/DtKWCYI2mWG.png?h=300&w=458 "(+)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXAN-1-OL")
Compound IX (+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-(PARA-METHOXYPHENYLCARBAMOYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANAL
![(+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-(PARA-METHOXYPHENYLCARBAMOYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANAL](/api/compound/38vYbAXBoht.png?h=300&w=458 "(+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-(PARA-METHOXYPHENYLCARBAMOYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANAL")
Compound V (-)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-(PARA-METHOXYPHENYLCARBAMOYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANAL
![(-)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-(PARA-METHOXYPHENYLCARBAMOYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANAL](/api/compound/8rir1WmHvy2.png?h=300&w=458 "(-)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-(PARA-METHOXYPHENYLCARBAMOYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANAL")
Compound VI (-)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-CARBAMOYL-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANOIC-ACID
![(-)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-CARBAMOYL-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANOIC-ACID](/api/compound/1OcAPKexQ8I.png?h=300&w=458 "(-)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-CARBAMOYL-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANOIC-ACID")
Compound VII (+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXAN-1-OL
![(+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXAN-1-OL](/api/compound/3D99uFRhfZs.png?h=300&w=458 "(+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXAN-1-OL")
Compound VIII (+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANAL
![(+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANAL](/api/compound/C1q1oJrU0Y1.png?h=300&w=458 "(+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANAL")
Compound X (+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-CARBAMOYL-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANOIC-ACID
![(+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-CARBAMOYL-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANOIC-ACID](/api/compound/9KCErpQXFoo.png?h=300&w=458 "(+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-CARBAMOYL-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANOIC-ACID")
Compound 5 GUADINOMIC_ACID
Compound 5 (-)-(5R,4'S)-6-(1'-CARBAMOYL-2'-IMINOIMIDAZOLIDIN-4'-YL)-5-HYDROXYHEXANOIC-ACID;(+)-(5R,4'S)-K01-0509-B
Compound 6 (-)-(5R,4'R)-6-[N,3-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXYLOXY-TERT.-BUTYLDIMETHYLSILANE
![(-)-(5R,4'R)-6-[N,3-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXYLOXY-TERT.-BUTYLDIMETHYLSILANE](/api/compound/E08jDdM98LD.png?h=300&w=458 "(-)-(5R,4'R)-6-[N,3-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXYLOXY-TERT.-BUTYLDIMETHYLSILANE")
Compound 7 (-)-(2S,4R)-1-[N',N''-BIS-(TERT.-BUTOXYCARBONYL)-GUANIDINO]-8-(TERT.-BUTYLDIMETHYLSILOXY)-4-(PARA-METHOXYBENZYLOXY)-OCTAN-2-OL
![(-)-(2S,4R)-1-[N',N''-BIS-(TERT.-BUTOXYCARBONYL)-GUANIDINO]-8-(TERT.-BUTYLDIMETHYLSILOXY)-4-(PARA-METHOXYBENZYLOXY)-OCTAN-2-OL](/api/compound/5iRZvyDkLsJ.png?h=300&w=458 "(-)-(2S,4R)-1-[N',N''-BIS-(TERT.-BUTOXYCARBONYL)-GUANIDINO]-8-(TERT.-BUTYLDIMETHYLSILOXY)-4-(PARA-METHOXYBENZYLOXY)-OCTAN-2-OL")
Compound 8 (-)-(2S,4R)-8-(TERT.-BUTYLDIMETHYLSILOXY)-4-(PARA-METHOXYBENZYLOXY)-1-NITROOCTAN-2-OL
Compound 9 (-)-(R)-7-(TERT.-BUTYLDIMETHYLSILOXY)-3-(PARA-METHOXYBENZYLOXY)-HEPTANAL
Compound 11 (-)-(2R,4R)-8-(TERT.-BUTYLDIMETHYLSILOXY)-4-(PARA-METHOXYBENZYLOXY)-1-NITROOCTAN-2-OL;MINOR-ISOMER
Compound 14 (+)-(R)-7-(TERT.-BUTYLDIMETHYLSILOXY)-HEPTANE-1,3-DIOL
Compound 15 (-)-(R)-7-(TERT.-BUTYLDIMETHYLSILOXY)-3-(PARA-METHOXYBENZYLOXY)-HEPTANOL
Compound 18 (-)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANAL
![(-)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANAL](/api/compound/jzgMtMVtoH.png?h=300&w=458 "(-)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANAL")
Compound 20 (-)-(2R,4R)-1-[N',N''-BIS-(TERT.-BUTOXYCARBONYL)-GUANIDINO]-8-(TERT.-BUTYLDIMETHYLSILOXY)-4-(PARA-METHOXYBENZYLOXY)-OCTAN-2-OL
![(-)-(2R,4R)-1-[N',N''-BIS-(TERT.-BUTOXYCARBONYL)-GUANIDINO]-8-(TERT.-BUTYLDIMETHYLSILOXY)-4-(PARA-METHOXYBENZYLOXY)-OCTAN-2-OL](/api/compound/qUQrhPzVC5.png?h=300&w=458 "(-)-(2R,4R)-1-[N',N''-BIS-(TERT.-BUTOXYCARBONYL)-GUANIDINO]-8-(TERT.-BUTYLDIMETHYLSILOXY)-4-(PARA-METHOXYBENZYLOXY)-OCTAN-2-OL")
Compound 21 (+)-(5S,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXYLOXY-TERT.-BUTYLDIMETHYLSILANE
![(+)-(5S,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXYLOXY-TERT.-BUTYLDIMETHYLSILANE](/api/compound/JwsepjHuMOv.png?h=300&w=458 "(+)-(5S,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXYLOXY-TERT.-BUTYLDIMETHYLSILANE")
#19;(-)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-(PARA-METHOXYPHENYLCARBAMOYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANOIC-ACID
![#19;(-)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-(PARA-METHOXYPHENYLCARBAMOYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANOIC-ACID](/api/compound/FBDaeqkRZSQ.png?h=300&w=458 "#19;(-)-(5R,4'R)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-(PARA-METHOXYPHENYLCARBAMOYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANOIC-ACID")
#22;(+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-(PARA-METHOXYPHENYLCARBAMOYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANOIC-ACID
![#22;(+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-(PARA-METHOXYPHENYLCARBAMOYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANOIC-ACID](/api/compound/5CkIKb4ePxL.png?h=300&w=458 "#22;(+)-(5R,4'S)-6-[N,3'-BIS-(TERT.-BUTOXYCARBONYL)-1'-(PARA-METHOXYPHENYLCARBAMOYL)-2'-IMINOIMIDAZOLIDIN-4'-YL]-5-(PARA-METHOXYBENZYLOXY)-HEXANOIC-ACID")
#II;(+)-(2S,4R)-N,N'-BIS-(TERT.-BUTOXYCARBONYL)-8-(TERT.-BUTYLDIMETHYLSILOXY)-4-(PARA-METHOXYBENZYLOXY)-2-[(S)-METHOXY-TRIFLUOROMETHYLPHENYLACETOXY]-GUANIDINE
![#II;(+)-(2S,4R)-N,N'-BIS-(TERT.-BUTOXYCARBONYL)-8-(TERT.-BUTYLDIMETHYLSILOXY)-4-(PARA-METHOXYBENZYLOXY)-2-[(S)-METHOXY-TRIFLUOROMETHYLPHENYLACETOXY]-GUANIDINE](/api/compound/4LvyavfIIag.png?h=300&w=458 "#II;(+)-(2S,4R)-N,N'-BIS-(TERT.-BUTOXYCARBONYL)-8-(TERT.-BUTYLDIMETHYLSILOXY)-4-(PARA-METHOXYBENZYLOXY)-2-[(S)-METHOXY-TRIFLUOROMETHYLPHENYLACETOXY]-GUANIDINE")
#III;(-)-(2S,4R)-N,N'-BIS-(TERT.-BUTOXYCARBONYL)-8-(TERT.-BUTYLDIMETHYLSILOXY)-4-(PARA-METHOXYBENZYLOXY)-2-[(R)-METHOXY-TRIFLUOROMETHYLPHENYLACETOXY]-GUANIDINE
![#III;(-)-(2S,4R)-N,N'-BIS-(TERT.-BUTOXYCARBONYL)-8-(TERT.-BUTYLDIMETHYLSILOXY)-4-(PARA-METHOXYBENZYLOXY)-2-[(R)-METHOXY-TRIFLUOROMETHYLPHENYLACETOXY]-GUANIDINE](/api/compound/1jYf0qMaJcF.png?h=300&w=458 "#III;(-)-(2S,4R)-N,N'-BIS-(TERT.-BUTOXYCARBONYL)-8-(TERT.-BUTYLDIMETHYLSILOXY)-4-(PARA-METHOXYBENZYLOXY)-2-[(R)-METHOXY-TRIFLUOROMETHYLPHENYLACETOXY]-GUANIDINE")
Citation
| Citation | ORG.LETTERS,8,5577(2006) |
|---|---|
| Journal | Organic Letters |
| Issue | 24 |
| Volume | 8 |
| Page(s) | 5577-5580 |
| Year | 2006 |
| Author(s) | Satoshi Tsuchiya, Toshiaki Sunazuka, Tomoyasu Hirose, Ryuma Mori, Toshiaki Tanaka, Masato Iwatsuki, Satoshi Ōmura |
| Publisher | American Chemical Society (ACS) |
| DOI | 10.1021/ol062282z |