Spectra for:
Claire Crawford, Adam Nelson, Ian Patel
Compound 2 (1S*,3R*,7R*,9S*,10S*,12R*,14R*)-10-HYDROXY-12-(2'-FORMYL)-ALLYL-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE
![(1S*,3R*,7R*,9S*,10S*,12R*,14R*)-10-HYDROXY-12-(2'-FORMYL)-ALLYL-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE](/api/compound/K9sktq24Yq1.png?h=300&w=458 "(1S*,3R*,7R*,9S*,10S*,12R*,14R*)-10-HYDROXY-12-(2'-FORMYL)-ALLYL-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE")
Compound 3 (1S*,3R*,7R*,9S*,14R*)-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADEC-10-ENE-12-ONE
![(1S*,3R*,7R*,9S*,14R*)-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADEC-10-ENE-12-ONE](/api/compound/Ci9pytb71N0.png?h=300&w=458 "(1S*,3R*,7R*,9S*,14R*)-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADEC-10-ENE-12-ONE")
Compound 4 (2R*,6R*/6S*,2'S*,3'R*,7'R*)-6-PIVALOYLOXY-2-(3'-HYDROXY-3'-METHYL-7'-PENTYLOXEPAN-2'-YLMETHYL)-6H-PYRAN-3-ONE;MAJOR-ISOMER
Compound 5 (1R*,5R*,7S*,9R*,10R*)-9-HYDROXY-1-METHYL-5-PENTYL-6,11,2'-TRIOXASPIROBICYCLO-[5.4.0]-UNDECANE-10,1'-CYCLOPENT-4'-ENE-3'-ONE
![(1R*,5R*,7S*,9R*,10R*)-9-HYDROXY-1-METHYL-5-PENTYL-6,11,2'-TRIOXASPIROBICYCLO-[5.4.0]-UNDECANE-10,1'-CYCLOPENT-4'-ENE-3'-ONE](/api/compound/jiVMGYS7HS.png?h=300&w=458 "(1R*,5R*,7S*,9R*,10R*)-9-HYDROXY-1-METHYL-5-PENTYL-6,11,2'-TRIOXASPIROBICYCLO-[5.4.0]-UNDECANE-10,1'-CYCLOPENT-4'-ENE-3'-ONE")
Compound 6A (2R*,2'S*,3'S*,7'S*)-2-(2'-FURAN-2-YL-2'-HYDROXYETHYL)-3-METHYL-7-PENTYLOXEPAN-3-OL
Compound 6B (2R*,2'R*,3'S*,7'S*)-2-(2'-FURAN-2-YL-2'-HYDROXYETHYL)-3-METHYL-7-PENTYLOXEPAN-3-OL
Compound 7 (2'S*,6'R*,3R*)-1-FURAN-2-YL-3-HYDROXY-3-(2'-METHYL-6'-PENTYLTETRAHYDROPYRAN-2'-YL)-PROPAN-1-ONE
Compound 9 (2R*,6S*)-2-METHOXY-2-METHYL-6-PENTYL-TETRAHYDROPYRAN
Compound 10 (2S*,6R*)-2-METHYL-6-PENTYL-2-PROPA-1',2'-DIENYL-TETRAHYDROPYRAN
Compound 11 (2S*,6R*)-2-METHYL-6-PENTYL-TETRAHYDROPYRAN-2-CARBOXALDEHYDE
Compound 15 (2'S*,3'R*,7'R*)-1-FURAN-2-YL-2-(3'-HYDROXY-3'-METHYL-7'-PENTYLOXEPAN-2-YL)-ETHANONE
Compound 16 (2R*,2'S*,3'S*,7'S*)-2-(2'-FURAN-2-YL-2'-TERT.-BUTYLDIMETHYLSILYLOXYETHYL)-3-METHYL-7-PENTYLOXEPAN-3-OL
Compound 18 (1S*,3R*,7R*,9S*,14R*)-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE-12-ONE
![(1S*,3R*,7R*,9S*,14R*)-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE-12-ONE](/api/compound/66tcA2woBpe.png?h=300&w=458 "(1S*,3R*,7R*,9S*,14R*)-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE-12-ONE")
Compound 19 (1S*,3R*,7R*,9S*,15R*)-7-METHYL-3-PENTYL-2,8,11,14-TETRAOXATETRACYCLO-[9.5.0.0(10,12)0(9,15)]-HEXADECAN-13-ONE
![(1S*,3R*,7R*,9S*,15R*)-7-METHYL-3-PENTYL-2,8,11,14-TETRAOXATETRACYCLO-[9.5.0.0(10,12)0(9,15)]-HEXADECAN-13-ONE](/api/compound/CKjptX7q551.png?h=300&w=458 "(1S*,3R*,7R*,9S*,15R*)-7-METHYL-3-PENTYL-2,8,11,14-TETRAOXATETRACYCLO-[9.5.0.0(10,12)0(9,15)]-HEXADECAN-13-ONE")
Compound 20 (1S*,3R*,7R*,9S*,10S*,14R*)-10-HYDROXY-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE-12-ONE
![(1S*,3R*,7R*,9S*,10S*,14R*)-10-HYDROXY-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE-12-ONE](/api/compound/5yaAp4sIcn4.png?h=300&w=458 "(1S*,3R*,7R*,9S*,10S*,14R*)-10-HYDROXY-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE-12-ONE")
Compound 21 (1S*,3R*,7R*,9S*,10S*,12R*/12S*14R*)-10-HYDROXY-12-METHOXY-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE;MAJOR-ISOMER
![(1S*,3R*,7R*,9S*,10S*,12R*/12S*14R*)-10-HYDROXY-12-METHOXY-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE;MAJOR-ISOMER](/api/compound/Ckgh9AdB5P2.png?h=300&w=458 "(1S*,3R*,7R*,9S*,10S*,12R*/12S*14R*)-10-HYDROXY-12-METHOXY-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE;MAJOR-ISOMER")
Compound 24 (1S*,3R*,7R*,9S*,10S*,12R*,14R*)-12-ACETOXYALLYLMETHYL-10-HYDROXY-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE
![(1S*,3R*,7R*,9S*,10S*,12R*,14R*)-12-ACETOXYALLYLMETHYL-10-HYDROXY-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE](/api/compound/H2EazpPGIGG.png?h=300&w=458 "(1S*,3R*,7R*,9S*,10S*,12R*,14R*)-12-ACETOXYALLYLMETHYL-10-HYDROXY-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE")
Compound 25 (1S*,3R*,7R*,9S*,10S*,12R*,14R*)-10-HYDROXY-12-HYDROXYALLYLMETHYL-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE
![(1S*,3R*,7R*,9S*,10S*,12R*,14R*)-10-HYDROXY-12-HYDROXYALLYLMETHYL-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE](/api/compound/9pDVHTO4W0e.png?h=300&w=458 "(1S*,3R*,7R*,9S*,10S*,12R*,14R*)-10-HYDROXY-12-HYDROXYALLYLMETHYL-7-METHYL-3-PENTYL-2,8,13-TRIOXATRICYCLO-[8.5.0.0(9,14)]-PENTADECANE")
Compound 26 (E)-(2'R*,6'S*)-1-FURAN-2-YL-3-(2'-METHYL-6'-PENTYLTETRAHYDROPYRAN-2'-YL)-PROPENONE
#17;(1R*,5R*,7S*,9R*,10R*)-9-TERT.-BUTYLDIMETHYLSILYLOXY-1-METHYL-5-PENTYL-6,11,2'-TRIOXASPIROBICYCLO-[5.4.0]-UNDECANE-10,1'-CYCLOPENT-4'-ENE-3'-ONE
![#17;(1R*,5R*,7S*,9R*,10R*)-9-TERT.-BUTYLDIMETHYLSILYLOXY-1-METHYL-5-PENTYL-6,11,2'-TRIOXASPIROBICYCLO-[5.4.0]-UNDECANE-10,1'-CYCLOPENT-4'-ENE-3'-ONE](/api/compound/5sSfnUd6EcU.png?h=300&w=458 "#17;(1R*,5R*,7S*,9R*,10R*)-9-TERT.-BUTYLDIMETHYLSILYLOXY-1-METHYL-5-PENTYL-6,11,2'-TRIOXASPIROBICYCLO-[5.4.0]-UNDECANE-10,1'-CYCLOPENT-4'-ENE-3'-ONE")
Citation
| Citation | ORG.LETTERS,8,4231(2006) |
|---|---|
| Journal | Organic Letters |
| Issue | 19 |
| Volume | 8 |
| Page(s) | 4231-4234 |
| Year | 2006 |
| Author(s) | Claire Crawford, Adam Nelson, Ian Patel |
| Publisher | American Chemical Society (ACS) |
| DOI | 10.1021/ol0614323 |