Spectra for:
Ali Sadeghi-Khomami, Alexander J. Blake, Claire Wilson, Neil R. Thomas
Compound 5 (+/-)-6-HYDROXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPT-2-EXO,3-ENDO-DIOL
![(+/-)-6-HYDROXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPT-2-EXO,3-ENDO-DIOL](/api/compound/DRiM6059ZM3.png?h=300&w=458 "(+/-)-6-HYDROXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPT-2-EXO,3-ENDO-DIOL")
Compound 6 (+/-)-7-OXA-BICYCLO-[2.2.1]-HEPT-5-ENE-TRANS-2,3-DICARBOXYLIC-ACID-DIMETHYLESTER
![(+/-)-7-OXA-BICYCLO-[2.2.1]-HEPT-5-ENE-TRANS-2,3-DICARBOXYLIC-ACID-DIMETHYLESTER](/api/compound/Jr6TMwburO0.png?h=300&w=458 "(+/-)-7-OXA-BICYCLO-[2.2.1]-HEPT-5-ENE-TRANS-2,3-DICARBOXYLIC-ACID-DIMETHYLESTER")
Compound 7 (+/-)-EXO-5,6-EPOXY-7-OXA-BICYCLO-[2.2.1]-HEPTAN-TRANS-2,3-DICARBOXYLIC-ACID-DIMETHYLESTER
![(+/-)-EXO-5,6-EPOXY-7-OXA-BICYCLO-[2.2.1]-HEPTAN-TRANS-2,3-DICARBOXYLIC-ACID-DIMETHYLESTER](/api/compound/JXq0wMSvf5K.png?h=300&w=458 "(+/-)-EXO-5,6-EPOXY-7-OXA-BICYCLO-[2.2.1]-HEPTAN-TRANS-2,3-DICARBOXYLIC-ACID-DIMETHYLESTER")
Compound 8 (+/-)-2-EXO-HYDROXY-5-OXO-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-9-EXO-CARBOXYLIC-ACID
![(+/-)-2-EXO-HYDROXY-5-OXO-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-9-EXO-CARBOXYLIC-ACID](/api/compound/2KA4vvE7ScY.png?h=300&w=458 "(+/-)-2-EXO-HYDROXY-5-OXO-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-9-EXO-CARBOXYLIC-ACID")
Compound 9 (+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-5-OXO-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-9-EXO-CARBOXYLIC-ACID
![(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-5-OXO-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-9-EXO-CARBOXYLIC-ACID](/api/compound/7G3BhMp5Mqt.png?h=300&w=458 "(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-5-OXO-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-9-EXO-CARBOXYLIC-ACID")
Compound 10 (+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-9-EXO-HYDROXYMETHYL-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-5-ONE
![(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-9-EXO-HYDROXYMETHYL-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-5-ONE](/api/compound/KzaV6GSkT9s.png?h=300&w=458 "(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-9-EXO-HYDROXYMETHYL-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-5-ONE")
Compound 11 (+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-9-EXO-HYDROXYMETHYL-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-5-OL
![(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-9-EXO-HYDROXYMETHYL-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-5-OL](/api/compound/7k9Ki49T7w5.png?h=300&w=458 "(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-9-EXO-HYDROXYMETHYL-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-5-OL")
Compound 12 (+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-5-ENDO,6-EXO-BISHYDROXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-3-OL
![(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-5-ENDO,6-EXO-BISHYDROXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-3-OL](/api/compound/4U18CTFQH8k.png?h=300&w=458 "(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-5-ENDO,6-EXO-BISHYDROXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-3-OL")
Compound 15 (+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-3-ENDO-ACETYL-6-EXO-ACETOXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-5-YLCARBOXALDEHYDE
![(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-3-ENDO-ACETYL-6-EXO-ACETOXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-5-YLCARBOXALDEHYDE](/api/compound/2z4PGtaz2sO.png?h=300&w=458 "(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-3-ENDO-ACETYL-6-EXO-ACETOXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-5-YLCARBOXALDEHYDE")
Compound 16 (+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-3-ENDO-ACETYL-6-EXO-ACETOXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-5-YLCARBOXYLIC-ACID
![(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-3-ENDO-ACETYL-6-EXO-ACETOXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-5-YLCARBOXYLIC-ACID](/api/compound/JzfKJuWjbGI.png?h=300&w=458 "(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-3-ENDO-ACETYL-6-EXO-ACETOXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-5-YLCARBOXYLIC-ACID")
Compound 17 (+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-6-EXO-ACETOXYMETHYL-3-ENDO-ACETOXY-7-OXA-BICYCLO-[2.2.1]-HEPTANE
![(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-6-EXO-ACETOXYMETHYL-3-ENDO-ACETOXY-7-OXA-BICYCLO-[2.2.1]-HEPTANE](/api/compound/JjlD2rLpm7o.png?h=300&w=458 "(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-6-EXO-ACETOXYMETHYL-3-ENDO-ACETOXY-7-OXA-BICYCLO-[2.2.1]-HEPTANE")
Compound 18 (+/-)-6-EXO-ACETOXYMETHYL-3-ENDO-ACETOXY-2-EXO-HYDROXY-7-OXA-BICYCLO-[2.2.1]-HEPTANE
![(+/-)-6-EXO-ACETOXYMETHYL-3-ENDO-ACETOXY-2-EXO-HYDROXY-7-OXA-BICYCLO-[2.2.1]-HEPTANE](/api/compound/LqEVdV9AHuQ.png?h=300&w=458 "(+/-)-6-EXO-ACETOXYMETHYL-3-ENDO-ACETOXY-2-EXO-HYDROXY-7-OXA-BICYCLO-[2.2.1]-HEPTANE")
Compound 19 (+/-)-6-EXO-ACETOXYMETHYL-2-EXO-ACETOXY-3-ENDO-HYDROXY-7-OXA-BICYCLO-[2.2.1]-HEPTANE
![(+/-)-6-EXO-ACETOXYMETHYL-2-EXO-ACETOXY-3-ENDO-HYDROXY-7-OXA-BICYCLO-[2.2.1]-HEPTANE](/api/compound/Wx9GWxUq2k.png?h=300&w=458 "(+/-)-6-EXO-ACETOXYMETHYL-2-EXO-ACETOXY-3-ENDO-HYDROXY-7-OXA-BICYCLO-[2.2.1]-HEPTANE")
Compound 20 (+/-)-6-EXO-ACETOXYMETHYL-2,3-TRANS-ACETOXY-7-OXA-BICYCLO-[2.2.1]-HEPTANE
![(+/-)-6-EXO-ACETOXYMETHYL-2,3-TRANS-ACETOXY-7-OXA-BICYCLO-[2.2.1]-HEPTANE](/api/compound/3fp7gwHjjH2.png?h=300&w=458 "(+/-)-6-EXO-ACETOXYMETHYL-2,3-TRANS-ACETOXY-7-OXA-BICYCLO-[2.2.1]-HEPTANE")
#13;(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-6-EXO-(TERT.-BUTYL-DIMETHYL-SILANYLOXYMETHYL)-5-ENDO-HYDROXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-3-ENDO-OL
![#13;(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-6-EXO-(TERT.-BUTYL-DIMETHYL-SILANYLOXYMETHYL)-5-ENDO-HYDROXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-3-ENDO-OL](/api/compound/DL4rKCw356.png?h=300&w=458 "#13;(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-6-EXO-(TERT.-BUTYL-DIMETHYL-SILANYLOXYMETHYL)-5-ENDO-HYDROXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-3-ENDO-OL")
#14;(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-3-ENDO-ACETYL-6-EXO-ACETOXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-5-YLCARBOXALDEHYDE-1,1-DIMETHYLHYDRAZONE
![#14;(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-3-ENDO-ACETYL-6-EXO-ACETOXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-5-YLCARBOXALDEHYDE-1,1-DIMETHYLHYDRAZONE](/api/compound/7p5FWCTKvvl.png?h=300&w=458 "#14;(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-3-ENDO-ACETYL-6-EXO-ACETOXYMETHYL-7-OXA-BICYCLO-[2.2.1]-HEPTAN-5-YLCARBOXALDEHYDE-1,1-DIMETHYLHYDRAZONE")
(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-9-EXO-TERT.-BUTYL-DIMETHYL-SILANYLOXYMETHYL-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-5-ONE
![(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-9-EXO-TERT.-BUTYL-DIMETHYL-SILANYLOXYMETHYL-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-5-ONE](/api/compound/HMvUW7M8w9t.png?h=300&w=458 "(+/-)-2-EXO-(TERT.-BUTYL-DIPHENYL-SILANYLOXY)-9-EXO-TERT.-BUTYL-DIMETHYL-SILANYLOXYMETHYL-4,8-DIOXA-TRICYCLO-[4.2.1.0(3,7)]-NONAN-5-ONE")
Citation
| Citation | ORG.LETTERS,7,4891(2005) |
|---|---|
| Journal | Organic Letters |
| Issue | 22 |
| Volume | 7 |
| Page(s) | 4891-4894 |
| Year | 2005 |
| Author(s) | Ali Sadeghi-Khomami, Alexander J. Blake, Claire Wilson, Neil R. Thomas |
| Publisher | American Chemical Society (ACS) |
| DOI | 10.1021/ol0517877 |