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Spectra for:
C. González-Bello, M. K. Manthey, J. H. Harris, A. R. Hawkins, J. R. Coggins, C. Abell

Compound 1 4 METHYL-(1S,5R)-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,5-DIHYDROXY-4-OXOCYCLOHEX-2-ENECARBOXYLATE

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METHYL-(1S,5R)-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,5-DIHYDROXY-4-OXOCYCLOHEX-2-ENECARBOXYLATE
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13C NMR Spectrum

Compound 5 (4S,5R)-2-BROMO-4,5-DIHYDROXY-3-OXOCYCLOHEX-1-ENE-CARBOXYLIC-ACID

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(4S,5R)-2-BROMO-4,5-DIHYDROXY-3-OXOCYCLOHEX-1-ENE-CARBOXYLIC-ACID
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13C NMR Spectrum

Compound 6 (4S,5R)-2-FLUORO-4,5-DIHYDROXY-3-OXOCYCLOHEX-1-ENE-CARBOXYLIC-ACID

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(4S,5R)-2-FLUORO-4,5-DIHYDROXY-3-OXOCYCLOHEX-1-ENE-CARBOXYLIC-ACID
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19F NMR Spectrum

Compound 8 (3S,4S,5R)-2-BROMO-3,4,5-TRIHYDROXYCYCLOHEX-1-ENE-CARBOXYLIC-ACID;2-BROMOSHIKIMIC-ACID

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(3S,4S,5R)-2-BROMO-3,4,5-TRIHYDROXYCYCLOHEX-1-ENE-CARBOXYLIC-ACID;2-BROMOSHIKIMIC-ACID
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13C NMR Spectrum

Compound 9 (3S,4S,5R)-2-FLUORO-3,4,5-TRIHYDROXYCYCLOHEX-1-ENE-CARBOXYLIC-ACID;2-FLUOROSHIKIMIC-ACID

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(3S,4S,5R)-2-FLUORO-3,4,5-TRIHYDROXYCYCLOHEX-1-ENE-CARBOXYLIC-ACID;2-FLUOROSHIKIMIC-ACID
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19F NMR Spectrum

Compound 12 METHYL-(1S,2R,4S,5R)-2-BROMO-4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,5-DIHYDROXY-3-OXOCYCLOHEXANECARBOXYLATE

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METHYL-(1S,2R,4S,5R)-2-BROMO-4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,5-DIHYDROXY-3-OXOCYCLOHEXANECARBOXYLATE
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13C NMR Spectrum

Compound 13 METHYL-(1S,2R,4S,5R)-4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,2-EPOXY-1,5-DIHYDROXY-3-OXOCYCLOHEXANECARBOXYLATE

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METHYL-(1S,2R,4S,5R)-4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,2-EPOXY-1,5-DIHYDROXY-3-OXOCYCLOHEXANECARBOXYLATE
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13C NMR Spectrum

Compound 15 METHYL-(4S,5R)-2-BROMO-4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-5-(TRIFLUOROACETYL)-3-OXOCYCLOHEX-1-ENECARBOXYLATE

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METHYL-(4S,5R)-2-BROMO-4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-5-(TRIFLUOROACETYL)-3-OXOCYCLOHEX-1-ENECARBOXYLATE
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13C NMR Spectrum

Compound 16 METHYL-(4S,5R)-2-BROMO-4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-5-HYDROXY-3-OXOCYCLOHEX-1-ENECARBOXYLATE

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METHYL-(4S,5R)-2-BROMO-4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-5-HYDROXY-3-OXOCYCLOHEX-1-ENECARBOXYLATE
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13C NMR Spectrum

Compound 17 METHYL-(4S,5R)-2-BROMO-4,5-DIHYDROXY-3-OXOCYCLOHEX-1-ENECARBOXYLATE

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METHYL-(4S,5R)-2-BROMO-4,5-DIHYDROXY-3-OXOCYCLOHEX-1-ENECARBOXYLATE
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13C NMR Spectrum

Compound 18 PARA-METHOXYBENZYL-(1S,2R,4S,5R)-2-BROMO-4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,5-DIHYDROXY-3-OXOCYCLOHEXANECARBOXYLATE

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PARA-METHOXYBENZYL-(1S,2R,4S,5R)-2-BROMO-4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1,5-DIHYDROXY-3-OXOCYCLOHEXANECARBOXYLATE
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13C NMR Spectrum

Compound 19 PARA-METHOXYBENZYL-(4S,5R)-2-BROMO-4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-5-(TRIFLUOROACETYL)-3-OXOCYCLOHEX-1-ENECARBOXYLATE

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PARA-METHOXYBENZYL-(4S,5R)-2-BROMO-4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-5-(TRIFLUOROACETYL)-3-OXOCYCLOHEX-1-ENECARBOXYLATE
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13C NMR Spectrum

Compound 20 PARA-METHOXYBENZYL-(4S,5R)-2-BROMO-4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-5-HYDROXY-3-OXOCYCLOHEX-1-ENECARBOXYLATE

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PARA-METHOXYBENZYL-(4S,5R)-2-BROMO-4-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-5-HYDROXY-3-OXOCYCLOHEX-1-ENECARBOXYLATE
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13C NMR Spectrum

METHYL-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-GALLATE

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METHYL-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-GALLATE
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13C NMR Spectrum

Citation

Citation J.ORG.CHEM.,63,1591(1998)
Journal The Journal of Organic Chemistry
Issue 5
Volume 63
Page(s) 1591-1597
Year 1998
Author(s) C. González-Bello, M. K. Manthey, J. H. Harris, A. R. Hawkins, J. R. Coggins, C. Abell
Publisher American Chemical Society (ACS)
DOI 10.1021/jo971858i