Spectra for:
Michael Meldgaard, Flemming Gundorph Hansen, Jesper Wengel
Compound 5 3-C-ALLYL-3-O-BENZYL-1,2:5,6-DI-O-ISOPROPYLIDENE-ALPHA-D-ALLOFURANOSE
Compound 6 3-C-ALLYL-3-O-BENZYL-4-C-HYDROXYMETHYL-1,2-O-ISOPROPYLIDENE-ALPHA-D-ERYTHROPENTOFURANOSE
Compound 7 4-C-ACETOXYMETHYL-5-O-ACETYL-3-C-ALLYL-3-O-BENZYL-1,2-O-ISOPROPYLIDENE-ALPHA-D-ERYTHROPENTOFURANOSE
Compound 8 4-C-ACETOXYMETHYL-3-C-ALLYL-3-O-BENZYL-1,2,5-TRI-O-ACETYL-D-ERYTHROPENTOFURANOSE
Compound 9 1-(4-C-ACETOXYMETHYL-3-C-ALLYL-3-O-BENZYL-2,5-DI-O-ACETYL-BETA-D-ERYTHROPENTOFURANOSYL)-THYMINE
Compound 10 1-(3-C-ALLYL-3-O-BENZYL-4-C-HYDROXYMETHYL-BETA-D-ERYTHROPENTOFURANOSYL)-THYMINE
Compound 11 1-(3-C-ALLYL-3-O-BENZYL-4-C-TOSYLOXYMETHYL-BETA-D-RIBOFURANOSYL)-THYMINE
Compound 12 1-[3-C-ALLYL-3-O-BENZYL-4-C-TOSYLOXYMETHYL-5-O-(4,4'-DIMETHOXYTRITYL)-BETA-D-RIBOFURANOSYL]-THYMINE
![1-[3-C-ALLYL-3-O-BENZYL-4-C-TOSYLOXYMETHYL-5-O-(4,4'-DIMETHOXYTRITYL)-BETA-D-RIBOFURANOSYL]-THYMINE](/api/compound/9Wrd1wsxjke.png?h=300&w=458 "1-[3-C-ALLYL-3-O-BENZYL-4-C-TOSYLOXYMETHYL-5-O-(4,4'-DIMETHOXYTRITYL)-BETA-D-RIBOFURANOSYL]-THYMINE")
Compound 13 (1R,3R,4R,7S)-7-ALLYL-7-BENZYLOXY-1-(4',4'-DIMETHOXYTRITYL)-OXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE
![(1R,3R,4R,7S)-7-ALLYL-7-BENZYLOXY-1-(4',4'-DIMETHOXYTRITYL)-OXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE](/api/compound/GgLSDDJTUC0.png?h=300&w=458 "(1R,3R,4R,7S)-7-ALLYL-7-BENZYLOXY-1-(4',4'-DIMETHOXYTRITYL)-OXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE")
Compound 14 (1R,3R,4R,7S)-7-BENZYLOXY-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-(2-HYDROXYMETHYL)-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE
![(1R,3R,4R,7S)-7-BENZYLOXY-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-(2-HYDROXYMETHYL)-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE](/api/compound/DPgYE5DzZ6t.png?h=300&w=458 "(1R,3R,4R,7S)-7-BENZYLOXY-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-(2-HYDROXYMETHYL)-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE")
Compound 15 (1R,3R,4R,7S)-1-(4',4'-DIMETHOXYTRITYL)-OXYMETHYL-7-HYDROXY-7-(2-HYDROXYMETHYL)-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE
![(1R,3R,4R,7S)-1-(4',4'-DIMETHOXYTRITYL)-OXYMETHYL-7-HYDROXY-7-(2-HYDROXYMETHYL)-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE](/api/compound/I0hgR4uJDzm.png?h=300&w=458 "(1R,3R,4R,7S)-1-(4',4'-DIMETHOXYTRITYL)-OXYMETHYL-7-HYDROXY-7-(2-HYDROXYMETHYL)-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE")
Compound 16 (1R,3R,4R,7S)-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-HYDROXY-7-(2-LEVULINOYLOXYETHYL)-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE
![(1R,3R,4R,7S)-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-HYDROXY-7-(2-LEVULINOYLOXYETHYL)-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE](/api/compound/A2pbNwIG2eE.png?h=300&w=458 "(1R,3R,4R,7S)-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-HYDROXY-7-(2-LEVULINOYLOXYETHYL)-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE")
Compound 18 1,2:5,6-DI-O-ISOPROPYLIDENE-3-C-(3-HYDROXY)-PROPYL-ALPHA-D-ALLOFURANOSE
Compound 19 3-O-BENZYL-3-C-(3-BENZYLOXY)-PROPYL-1,2-O-ISOPROPYLIDENE-ALPHA-D-ALLOFURANOSE
Compound 20 3-O-BENZYL-3-C-(3-BENZYLOXY)-PROPYL-4-C-HYDROXYMETHYL-1,2-O-ISOPROPYLIDENE-ALPHA-D-ERYTHRO-PENTOFURANOSE
Compound 21 1,2-DI-O-ACETYL-3-O-BENZYL-3-C-(3-BENZYLOXY)-PROPYL-4-O-MESYL-4-C-MESYLOXYMETHYL-D-ERYTHRO-PENTOFURANOSE
Compound 22 1-(2-O-ACETYL-3-O-BENZYL-3-C-(3-BENZYLOXY)-PROPYL-5-O-MESYL-4-C-HYDROXYMETHYL-BETA-D-ERYTHRO-PENTOFURANOSYL)-THYMINE
Compound 23 (1S,3R,4R,7S)-7-BENZYLOXY-7-(3-BENZYLOXY)-PROPYL-1-HYDROXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE
![(1S,3R,4R,7S)-7-BENZYLOXY-7-(3-BENZYLOXY)-PROPYL-1-HYDROXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE](/api/compound/9vcmOZQhcQe.png?h=300&w=458 "(1S,3R,4R,7S)-7-BENZYLOXY-7-(3-BENZYLOXY)-PROPYL-1-HYDROXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE")
Compound 24 (1R,3R,4R,7S)-7-BENZYLOXY-7-(3-BENZYLOXY)-PROPYL-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE
![(1R,3R,4R,7S)-7-BENZYLOXY-7-(3-BENZYLOXY)-PROPYL-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE](/api/compound/JpJgnTq9tox.png?h=300&w=458 "(1R,3R,4R,7S)-7-BENZYLOXY-7-(3-BENZYLOXY)-PROPYL-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE")
Compound 25 (1R,3R,4R,7S)-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-HYDROXY-7-(3-HYDROXY)-PROPYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE
![(1R,3R,4R,7S)-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-HYDROXY-7-(3-HYDROXY)-PROPYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE](/api/compound/9BNuTQlHcIs.png?h=300&w=458 "(1R,3R,4R,7S)-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-HYDROXY-7-(3-HYDROXY)-PROPYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE")
Compound 26 (1R,3R,4R,7S)-7-(3-ACETOXYPROPYL)-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-HYDROXY-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE
![(1R,3R,4R,7S)-7-(3-ACETOXYPROPYL)-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-HYDROXY-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE](/api/compound/472nbhuXUHn.png?h=300&w=458 "(1R,3R,4R,7S)-7-(3-ACETOXYPROPYL)-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-HYDROXY-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE")
Compound 28 3-O-BENZYL-1,2:5,6-DI-O-ISOPROPYLIDENE-3-C-(3-HYDROXY)-PROPYL-ALPHA-D-ALLOFURANOSE
Compound 29 3-O-BENZYL-1,2:5,6-DI-O-ISOPROPYLIDENE-3-C-(3-MESYLOXY)-PROPYL-ALPHA-D-ALLOFURANOSE
Compound 30 3-C-(3-AZIDOPROPYL)-3-O-BENZYL-1,2:5,6-DI-O-ISOPROPYLIDENE-ALPHA-D-ALLOFURANOSE
Compound 31 3-C-(3-AZIDO)-PROPYL-3-O-BENZYL-1,2-O-ISOPROPYLIDENE-ALPHA-D-ALLOFURANOSE
Compound 32 3-C-(3-AZIDOPROPYL)-3-O-BENZYL-4-C-HYDROXYMETHYL-1,2-O-ISOPROPYLIDENE-ALPHA-D-ERYTHRO-PENTOFURANOSE
Compound 33 3-C-(3-AZIDOPROPYL)-1,2-DI-O-ACETYL-3-O-BENZYL-5-O-MESYL-4-C-MESYLOXYMETHYL-D-ERYTHRO-PENTOFURANOSE
Compound 34 1-[2-O-ACETYL-3-C-(3-AZIDOPROPYL)-3-O-BENZYL-5-O-MESYL-4-C-MESYLOXYMETHYL-BETA-D-ERYTHRO-PENTOFURANOSYL]-THYMINE
![1-[2-O-ACETYL-3-C-(3-AZIDOPROPYL)-3-O-BENZYL-5-O-MESYL-4-C-MESYLOXYMETHYL-BETA-D-ERYTHRO-PENTOFURANOSYL]-THYMINE](/api/compound/7oFQcndysj2.png?h=300&w=458 "1-[2-O-ACETYL-3-C-(3-AZIDOPROPYL)-3-O-BENZYL-5-O-MESYL-4-C-MESYLOXYMETHYL-BETA-D-ERYTHRO-PENTOFURANOSYL]-THYMINE")
Compound 35 (1S,3R,4R,7S)-7-(3-AZIDOPROPYL)-7-BENZYLOXY-1-HYDROXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE
![(1S,3R,4R,7S)-7-(3-AZIDOPROPYL)-7-BENZYLOXY-1-HYDROXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE](/api/compound/CcAjk1H9VNf.png?h=300&w=458 "(1S,3R,4R,7S)-7-(3-AZIDOPROPYL)-7-BENZYLOXY-1-HYDROXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE")
Compound 36 (1S,3R,4R,7S)-7-[3-(FLUOREN-9-YLMETHOXYCARBONYL)-AMINOPROPYL]-7-HYDROXY-1-HYDROXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE
![(1S,3R,4R,7S)-7-[3-(FLUOREN-9-YLMETHOXYCARBONYL)-AMINOPROPYL]-7-HYDROXY-1-HYDROXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE](/api/compound/HSzzqsSDFgA.png?h=300&w=458 "(1S,3R,4R,7S)-7-[3-(FLUOREN-9-YLMETHOXYCARBONYL)-AMINOPROPYL]-7-HYDROXY-1-HYDROXYMETHYL-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTANE")
#17;(1R,3R,4R,7S)-7-(2-Levulinoyloxy)-ethyl-(2-cyanoethoxy)-[N,N-(diisopropyl)-amino]-phosphinoxy-1-(4,4'-dimethoxytrityl)-oxymethyl-3-(thymin-1-yl)-2,5-dioxab
![#17;(1R,3R,4R,7S)-7-(2-Levulinoyloxy)-ethyl-(2-cyanoethoxy)-[N,N-(diisopropyl)-amino]-phosphinoxy-1-(4,4'-dimethoxytrityl)-oxymethyl-3-(thymin-1-yl)-2,5-dioxab](/api/compound/2vcE7NbrkcX.png?h=300&w=458 "#17;(1R,3R,4R,7S)-7-(2-Levulinoyloxy)-ethyl-(2-cyanoethoxy)-[N,N-(diisopropyl)-amino]-phosphinoxy-1-(4,4'-dimethoxytrityl)-oxymethyl-3-(thymin-1-yl)-2,5-dioxab")
#27;(1R,3R,4R,7S)-7-(3-Acetoxypropyl)-7-(2-cyanoethoxy)-[N,N-(diisopropyl)-amino]-phosphinoxy-1-(4,4'-dimethoxytrityl)-oxymethyl-3-(thymin-1-yl)-2,5-dioxabicyc
![#27;(1R,3R,4R,7S)-7-(3-Acetoxypropyl)-7-(2-cyanoethoxy)-[N,N-(diisopropyl)-amino]-phosphinoxy-1-(4,4'-dimethoxytrityl)-oxymethyl-3-(thymin-1-yl)-2,5-dioxabicyc](/api/compound/DHGHBQsbAte.png?h=300&w=458 "#27;(1R,3R,4R,7S)-7-(3-Acetoxypropyl)-7-(2-cyanoethoxy)-[N,N-(diisopropyl)-amino]-phosphinoxy-1-(4,4'-dimethoxytrityl)-oxymethyl-3-(thymin-1-yl)-2,5-dioxabicyc")
#37;(1R,3R,4R,7S)-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-[3-(FLUOREN-9-YL-METHOXYCARBONYL)-AMINOPROPYL]-7-HYDROXY-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTAN
![#37;(1R,3R,4R,7S)-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-[3-(FLUOREN-9-YL-METHOXYCARBONYL)-AMINOPROPYL]-7-HYDROXY-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTAN](/api/compound/3A2hJlJbLvH.png?h=300&w=458 "#37;(1R,3R,4R,7S)-1-(4,4'-DIMETHOXYTRITYL)-OXYMETHYL-7-[3-(FLUOREN-9-YL-METHOXYCARBONYL)-AMINOPROPYL]-7-HYDROXY-3-(THYMIN-1-YL)-2,5-DIOXABICYCLO-[2.2.1]-HEPTAN")
#38;(1R,3R,4R,7S)-7-(2-Cyanoethoxy)-[N,N-(diisopropylamino)-phosphinoxy]-1-(4,4'-dimethoxytrityl)-oxymethyl-7-[3-(fluoren-9-yl-methoxycarbonyl)-amino]-propyl-3
![#38;(1R,3R,4R,7S)-7-(2-Cyanoethoxy)-[N,N-(diisopropylamino)-phosphinoxy]-1-(4,4'-dimethoxytrityl)-oxymethyl-7-[3-(fluoren-9-yl-methoxycarbonyl)-amino]-propyl-3](/api/compound/HsU0rK8WhoS.png?h=300&w=458 "#38;(1R,3R,4R,7S)-7-(2-Cyanoethoxy)-[N,N-(diisopropylamino)-phosphinoxy]-1-(4,4'-dimethoxytrityl)-oxymethyl-7-[3-(fluoren-9-yl-methoxycarbonyl)-amino]-propyl-3")
Citation
| Citation | J.ORG.CHEM.,69,6310(2004) |
|---|---|
| Journal | The Journal of Organic Chemistry |
| Issue | 19 |
| Volume | 69 |
| Page(s) | 6310-6322 |
| Year | 2004 |
| Author(s) | Michael Meldgaard, Flemming Gundorph Hansen, Jesper Wengel |
| Publisher | American Chemical Society (ACS) |
| DOI | 10.1021/jo049159a |