Spectra for:
Katsutoshi Suzuki, Toshio Fuchigami
Compound 1A (R)-4-[(PHENYLTHIO)-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE
![(R)-4-[(PHENYLTHIO)-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE](/api/compound/JWF1gNJZlXA.png?h=300&w=458 "(R)-4-[(PHENYLTHIO)-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE")
Compound 1B (R)-4-[[(PARA-CHLOROPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE
![(R)-4-[[(PARA-CHLOROPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE](/api/compound/L6QPTvm4ery.png?h=300&w=458 "(R)-4-[[(PARA-CHLOROPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE")
Compound 1C (R)-4-[[(PARA-NITROPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE
![(R)-4-[[(PARA-NITROPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE](/api/compound/IN31jBgWm7Z.png?h=300&w=458 "(R)-4-[[(PARA-NITROPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE")
Compound 1D (R)-4-[[(PARA-METHOXYPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE
![(R)-4-[[(PARA-METHOXYPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE](/api/compound/BtA4HzbXxfS.png?h=300&w=458 "(R)-4-[[(PARA-METHOXYPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE")
Compound 2A (R)-4-[FLUORO-(PHENYLTHIO)-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER
![(R)-4-[FLUORO-(PHENYLTHIO)-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER](/api/compound/KTkNdtrR33J.png?h=300&w=458 "(R)-4-[FLUORO-(PHENYLTHIO)-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER")
Compound 2B (R)-4-[FLUORO-[(PARA-CHLOROPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER
![(R)-4-[FLUORO-[(PARA-CHLOROPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER](/api/compound/DvhNUaYLVWv.png?h=300&w=458 "(R)-4-[FLUORO-[(PARA-CHLOROPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER")
Compound 2C (R)-4-[FLUORO-[(PARA-NITROPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER
![(R)-4-[FLUORO-[(PARA-NITROPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER](/api/compound/8WOnVGkFckH.png?h=300&w=458 "(R)-4-[FLUORO-[(PARA-NITROPHENYL)-THIO]-METHYL]-2-SPIRO-CYCLOHEXYL-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER")
Compound 3 2-METHOXYPROPYL-PHENYL-SULFIDE
Compound 4 2-METHOXY-1-FLUOROPROPYL-PHENYL-SULFIDE;LESS-POLAR-DIASTEREOMER
Compound 5 2,3-DIMETHOXYPROPYL-PHENYL-SULFIDE
Compound 6 2,3-DIMETHOXY-1-FLUOROPROPYL-PHENYL-SULFIDE;LESS-POLAR-DIASTEREOMER
Compound 7 1-[(PHENYLTHIO)-METHYL]-TETRAHYDROFURAN
![1-[(PHENYLTHIO)-METHYL]-TETRAHYDROFURAN](/api/compound/I34PgMbNdkg.png?h=300&w=458 "1-[(PHENYLTHIO)-METHYL]-TETRAHYDROFURAN")
Compound 8 1-[(PHENYLTHIO)-FLUOROMETHYL]-TETRAHYDROFURAN;LESS-POLAR-DIASTEREOMER
![1-[(PHENYLTHIO)-FLUOROMETHYL]-TETRAHYDROFURAN;LESS-POLAR-DIASTEREOMER](/api/compound/4xMUddLxrzT.png?h=300&w=458 "1-[(PHENYLTHIO)-FLUOROMETHYL]-TETRAHYDROFURAN;LESS-POLAR-DIASTEREOMER")
Compound 9 4-[(PHENYLTHIO)-METHYL]-1,3-DIOXOLANE
![4-[(PHENYLTHIO)-METHYL]-1,3-DIOXOLANE](/api/compound/HJU4YCvABp6.png?h=300&w=458 "4-[(PHENYLTHIO)-METHYL]-1,3-DIOXOLANE")
Compound 10 4-[FLUORO-(PHENYLTHIO)-METHYL]-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER
![4-[FLUORO-(PHENYLTHIO)-METHYL]-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER](/api/compound/Fq7FQw1O4ND.png?h=300&w=458 "4-[FLUORO-(PHENYLTHIO)-METHYL]-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER")
Compound 11 (R)-4-[(PHENYLTHIO)-METHYL]-2,2-DIMETHYL-1,3-DIOXOLANE
![(R)-4-[(PHENYLTHIO)-METHYL]-2,2-DIMETHYL-1,3-DIOXOLANE](/api/compound/KB7J1PNsBmb.png?h=300&w=458 "(R)-4-[(PHENYLTHIO)-METHYL]-2,2-DIMETHYL-1,3-DIOXOLANE")
Compound 12 (R)-4-[FLUORO-(PHENYLTHIO)-METHYL]-2,2-DIMETHYL-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER
![(R)-4-[FLUORO-(PHENYLTHIO)-METHYL]-2,2-DIMETHYL-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER](/api/compound/6IvA5u0NIVM.png?h=300&w=458 "(R)-4-[FLUORO-(PHENYLTHIO)-METHYL]-2,2-DIMETHYL-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER")
Compound 13 (R)-4-[(PHENYLTHIO)-METHYL]-2-(2-SPIROADAMANTYL)-1,3-DIOXOLANE
![(R)-4-[(PHENYLTHIO)-METHYL]-2-(2-SPIROADAMANTYL)-1,3-DIOXOLANE](/api/compound/HDlIz8PAJ3I.png?h=300&w=458 "(R)-4-[(PHENYLTHIO)-METHYL]-2-(2-SPIROADAMANTYL)-1,3-DIOXOLANE")
Compound 14 (R)-4-[FLUORO-(PHENYLTHIO)-METHYL]-2-(2-SPIROADAMANTYL)-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER
![(R)-4-[FLUORO-(PHENYLTHIO)-METHYL]-2-(2-SPIROADAMANTYL)-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER](/api/compound/I78JVsbwarM.png?h=300&w=458 "(R)-4-[FLUORO-(PHENYLTHIO)-METHYL]-2-(2-SPIROADAMANTYL)-1,3-DIOXOLANE;LESS-POLAR-DIASTEREOMER")
Compound 15 4-[(PHENYLTHIO)-METHYL]-1,3-DIOXOLAN-2-ONE
![4-[(PHENYLTHIO)-METHYL]-1,3-DIOXOLAN-2-ONE](/api/compound/JzrIJH1pzNC.png?h=300&w=458 "4-[(PHENYLTHIO)-METHYL]-1,3-DIOXOLAN-2-ONE")
Compound 16 4-[FLUORO-(PHENYLTHIO)-METHYL]-1,3-DIOXOLAN-2-ONE;LESS-POLAR-DIASTEREOMER
![4-[FLUORO-(PHENYLTHIO)-METHYL]-1,3-DIOXOLAN-2-ONE;LESS-POLAR-DIASTEREOMER](/api/compound/2oTS8KTNWH.png?h=300&w=458 "4-[FLUORO-(PHENYLTHIO)-METHYL]-1,3-DIOXOLAN-2-ONE;LESS-POLAR-DIASTEREOMER")
Compound 17 4-[[(PARA-NITROPHENYL)-THIO]-METHYL]-1,3-DIOXOLAN-2-ONE
![4-[[(PARA-NITROPHENYL)-THIO]-METHYL]-1,3-DIOXOLAN-2-ONE](/api/compound/LkTG3mW0EzM.png?h=300&w=458 "4-[[(PARA-NITROPHENYL)-THIO]-METHYL]-1,3-DIOXOLAN-2-ONE")
Compound 18 4-[FLUORO-[(PARA-NITROPHENYL)-THIO]-METHYL]-1,3-DIOXOLAN-2-ONE;LESS-POLAR-DIASTEREOMER
![4-[FLUORO-[(PARA-NITROPHENYL)-THIO]-METHYL]-1,3-DIOXOLAN-2-ONE;LESS-POLAR-DIASTEREOMER](/api/compound/9KSmEHT2KrN.png?h=300&w=458 "4-[FLUORO-[(PARA-NITROPHENYL)-THIO]-METHYL]-1,3-DIOXOLAN-2-ONE;LESS-POLAR-DIASTEREOMER")
Compound 19 (1R,2S)-4-[FLUORO-(PHENYLSULFONYL)-METHYL]-2-SPIROCYCLOHEXYL-1,3-DIOXOLANE
![(1R,2S)-4-[FLUORO-(PHENYLSULFONYL)-METHYL]-2-SPIROCYCLOHEXYL-1,3-DIOXOLANE](/api/compound/76xwECED8Fe.png?h=300&w=458 "(1R,2S)-4-[FLUORO-(PHENYLSULFONYL)-METHYL]-2-SPIROCYCLOHEXYL-1,3-DIOXOLANE")
Compound 20 (1R,2S)-3-FLUORO-3-(PHENYLSULFONYL)-1,2-PROPANEDIOL
Citation
| Citation | J.ORG.CHEM.,69,1276(2004) |
|---|---|
| Journal | The Journal of Organic Chemistry |
| Issue | 4 |
| Volume | 69 |
| Page(s) | 1276-1282 |
| Year | 2004 |
| Author(s) | Katsutoshi Suzuki, Toshio Fuchigami |
| Publisher | American Chemical Society (ACS) |
| DOI | 10.1021/jo035291j |