Spectra for:
Alessandro Dondoni, Alessandro Massi, Erik Minghini, Simona Sabbatini, Valerio Bertolasi
Compound 31 (4R,2'S)-4-(2'-AMINO-2'-METHOXYCARBONYL-ETHYL)-1,3-DI-N-BENZYL-6-METHYL-2-OXO-1,2,3,4-TETRAHYDRO-PYRIMIDINE-5-CARBOXYLIC-ACID-ETHYLESTER
Compound 32 (2'S)-4-(2'-AMINO-2'-METHOXYCARBONYL-ETHYL)-2,6-DIMETHYL-PYRIDINE-3,5-DICARBOXYLIC-ACID-DI-TERT.-BUTYLESTER
Compound 33 (2'S)-2-(2'-AMINO-2'-METHOXYCARBONYL-ETHYL)-6-METHYL-4-PHENYL-PYRIDINE-3,5-DICARBOXYLIC-ACID-DI-TERT.-BUTYLESTER
Compound 34 (3S)-6,8-DIMETHYL-1-OXO-1,2,3,4-TETRAHYDRO-[2.7]-NAPHTHYRIDINE-3,5-DICARBOXYLIC-ACID-DIMETHYLESTER
![(3S)-6,8-DIMETHYL-1-OXO-1,2,3,4-TETRAHYDRO-[2.7]-NAPHTHYRIDINE-3,5-DICARBOXYLIC-ACID-DIMETHYLESTER](/api/compound/5Ju6Y4YeBV9.png?h=300&w=458 "(3S)-6,8-DIMETHYL-1-OXO-1,2,3,4-TETRAHYDRO-[2.7]-NAPHTHYRIDINE-3,5-DICARBOXYLIC-ACID-DIMETHYLESTER")
#-(4R)-30-(R)-MOSHER-AMIDE;(4R,1'S,2''R)-1,3-DI-N-BENZYL-4-[METHOXYCARBONYL-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLAMINO)-METHYL]-6-METHYL-2-OXO-1,2,
![#-(4R)-30-(R)-MOSHER-AMIDE;(4R,1'S,2''R)-1,3-DI-N-BENZYL-4-[METHOXYCARBONYL-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLAMINO)-METHYL]-6-METHYL-2-OXO-1,2,](/api/compound/90kAVfu8dQW.png?h=300&w=458 "#-(4R)-30-(R)-MOSHER-AMIDE;(4R,1'S,2''R)-1,3-DI-N-BENZYL-4-[METHOXYCARBONYL-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLAMINO)-METHYL]-6-METHYL-2-OXO-1,2,")
#-(4R)-30-(S)-Mosher-amide;(4R,1'S,2''S)-1,3-di-N-benzyl-4-[methoxycarbonyl-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionylamino)-methyl]-6-methyl-2-oxo-1,2,
![#-(4R)-30-(S)-Mosher-amide;(4R,1'S,2''S)-1,3-di-N-benzyl-4-[methoxycarbonyl-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionylamino)-methyl]-6-methyl-2-oxo-1,2,](/api/compound/CtP7FRs4hZM.png?h=300&w=458 "#-(4R)-30-(S)-Mosher-amide;(4R,1'S,2''S)-1,3-di-N-benzyl-4-[methoxycarbonyl-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionylamino)-methyl]-6-methyl-2-oxo-1,2,")
#-(4R)-5-(R)-MOSHERESTER;(4R,1'S,2''R)-4-[1'-TERT.-BUTOXYCARBONYLAMINO-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLOXY)-ETHYL]-6-METHYL-2-OXO-1,
![#-(4R)-5-(R)-MOSHERESTER;(4R,1'S,2''R)-4-[1'-TERT.-BUTOXYCARBONYLAMINO-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLOXY)-ETHYL]-6-METHYL-2-OXO-1,](/api/compound/IVn00jzywMX.png?h=300&w=458 "#-(4R)-5-(R)-MOSHERESTER;(4R,1'S,2''R)-4-[1'-TERT.-BUTOXYCARBONYLAMINO-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLOXY)-ETHYL]-6-METHYL-2-OXO-1,")
#-(4R)-5-(S)-Mosherester;(4R,1'S,2''S)-4-[1'-tert.-butoxycarbonylamino-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionyloxy)-ethyl]-6-methyl-2-oxo-1,
![#-(4R)-5-(S)-Mosherester;(4R,1'S,2''S)-4-[1'-tert.-butoxycarbonylamino-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionyloxy)-ethyl]-6-methyl-2-oxo-1,](/api/compound/4TmH3PbdO7q.png?h=300&w=458 "#-(4R)-5-(S)-Mosherester;(4R,1'S,2''S)-4-[1'-tert.-butoxycarbonylamino-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionyloxy)-ethyl]-6-methyl-2-oxo-1,")
#-(4S)-31-(R)-MOSHER-AMIDE;(4S,2'S,2''R)-1,3-DI-N-BENZYL-4-[2'-METHOXYCARBONYL-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLAMINO)-ETHYL]-6-METHYL-2-OXO
![#-(4S)-31-(R)-MOSHER-AMIDE;(4S,2'S,2''R)-1,3-DI-N-BENZYL-4-[2'-METHOXYCARBONYL-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLAMINO)-ETHYL]-6-METHYL-2-OXO](/api/compound/CYto3F2qRTa.png?h=300&w=458 "#-(4S)-31-(R)-MOSHER-AMIDE;(4S,2'S,2''R)-1,3-DI-N-BENZYL-4-[2'-METHOXYCARBONYL-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLAMINO)-ETHYL]-6-METHYL-2-OXO")
#-(4S)-31-(S)-Mosher-amide;(4S,2'S,2''S)-1,3-di-N-benzyl-4-[2'-methoxycarbonyl-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionylamino)-ethyl]-6-methyl-2-oxo
![#-(4S)-31-(S)-Mosher-amide;(4S,2'S,2''S)-1,3-di-N-benzyl-4-[2'-methoxycarbonyl-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionylamino)-ethyl]-6-methyl-2-oxo](/api/compound/Hhg6bxplsqR.png?h=300&w=458 "#-(4S)-31-(S)-Mosher-amide;(4S,2'S,2''S)-1,3-di-N-benzyl-4-[2'-methoxycarbonyl-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionylamino)-ethyl]-6-methyl-2-oxo")
#-20-(R)-MOSHERESTER;MAJOR-DIASTEREOMER;(1'S,2''R)-4-[1'-TERT.-BUTOXYCARBONYLAMINO-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLOXY)-ETHYL]-2,6-D
![#-20-(R)-MOSHERESTER;MAJOR-DIASTEREOMER;(1'S,2''R)-4-[1'-TERT.-BUTOXYCARBONYLAMINO-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLOXY)-ETHYL]-2,6-D](/api/compound/A8j8m3Rug4R.png?h=300&w=458 "#-20-(R)-MOSHERESTER;MAJOR-DIASTEREOMER;(1'S,2''R)-4-[1'-TERT.-BUTOXYCARBONYLAMINO-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLOXY)-ETHYL]-2,6-D")
#-20-(R)-Mosherester;minor-diastereomer;(1'R,2''R)-4-[1'-tert.-butoxycarbonylamino-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionyloxy)-ethyl]-2,6-D
![#-20-(R)-Mosherester;minor-diastereomer;(1'R,2''R)-4-[1'-tert.-butoxycarbonylamino-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionyloxy)-ethyl]-2,6-D](/api/compound/82awzrn8IUx.png?h=300&w=458 "#-20-(R)-Mosherester;minor-diastereomer;(1'R,2''R)-4-[1'-tert.-butoxycarbonylamino-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionyloxy)-ethyl]-2,6-D")
#-32-(R)-MOSHER-AMIDE;(2'S,2''R)-4-[2'-METHOXYCARBONYL-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLAMINO)-ETHYL]-2,6-DIMETHYL-PYRIDINE-3,5-DICARBOXYLIC
![#-32-(R)-MOSHER-AMIDE;(2'S,2''R)-4-[2'-METHOXYCARBONYL-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLAMINO)-ETHYL]-2,6-DIMETHYL-PYRIDINE-3,5-DICARBOXYLIC](/api/compound/CnhByEcIJLH.png?h=300&w=458 "#-32-(R)-MOSHER-AMIDE;(2'S,2''R)-4-[2'-METHOXYCARBONYL-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLAMINO)-ETHYL]-2,6-DIMETHYL-PYRIDINE-3,5-DICARBOXYLIC")
#-32-(S)-Mosher-amide;(2'S,2''S)-4-[2'-methoxycarbonyl-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionylamino)-ethyl]-2,6-dimethyl-pyridine-3,5-dicarboxylic
![#-32-(S)-Mosher-amide;(2'S,2''S)-4-[2'-methoxycarbonyl-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionylamino)-ethyl]-2,6-dimethyl-pyridine-3,5-dicarboxylic](/api/compound/LlZjvTMzunW.png?h=300&w=458 "#-32-(S)-Mosher-amide;(2'S,2''S)-4-[2'-methoxycarbonyl-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionylamino)-ethyl]-2,6-dimethyl-pyridine-3,5-dicarboxylic")
#-33-(R)-MOSHER-AMIDE;(2'S,2''R)-2-[2'-METHOXYCARBONYL-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLAMINO)-ETHYL]-6-METHYL-4-PHENYL-PYRIDINE-3,5-DICARBO
![#-33-(R)-MOSHER-AMIDE;(2'S,2''R)-2-[2'-METHOXYCARBONYL-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLAMINO)-ETHYL]-6-METHYL-4-PHENYL-PYRIDINE-3,5-DICARBO](/api/compound/FQPce3C8hzO.png?h=300&w=458 "#-33-(R)-MOSHER-AMIDE;(2'S,2''R)-2-[2'-METHOXYCARBONYL-2'-(3'',3'',3''-TRIFLUORO-2''-METHOXY-2''-PHENYL-PROPIONYLAMINO)-ETHYL]-6-METHYL-4-PHENYL-PYRIDINE-3,5-DICARBO")
#-33-(S)-Mosher-amide;(2'S,2''S)-2-[2'-methoxycarbonyl-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionylamino)-ethyl]-6-methyl-4-phenyl-pyridine-3,5-dicarbo
![#-33-(S)-Mosher-amide;(2'S,2''S)-2-[2'-methoxycarbonyl-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionylamino)-ethyl]-6-methyl-4-phenyl-pyridine-3,5-dicarbo](/api/compound/5GAxAkPfqm1.png?h=300&w=458 "#-33-(S)-Mosher-amide;(2'S,2''S)-2-[2'-methoxycarbonyl-2'-(3'',3'',3''-trifluoro-2''-methoxy-2''-phenyl-propionylamino)-ethyl]-6-methyl-4-phenyl-pyridine-3,5-dicarbo")
Citation
| Citation | J.ORG.CHEM.,68,6172(2003) |
|---|---|
| Journal | The Journal of Organic Chemistry |
| Issue | 16 |
| Volume | 68 |
| Page(s) | 6172-6183 |
| Year | 2003 |
| Author(s) | Alessandro Dondoni, Alessandro Massi, Erik Minghini, Simona Sabbatini, Valerio Bertolasi |
| Publisher | American Chemical Society (ACS) |
| DOI | 10.1021/jo0342830 |