Spectra for:
Daniel Oves, Miguel Ferrero, Susana Fernández, Vicente Gotor
Compound 3-HCL 1-ALPHA-AMINO-25-HYDROXYVITAMIN-D3-HYDROCHLORIDE
Compound 4-HCL 3-BETA-AMINO-3-DEOXY-1-ALPHA,25-DIHYDROXYVITAMIN-D3-HYDROCHLORIDE
Compound 8 (1S,4S,6S)-1-METHYL-4-ISOPRENYL-7-AZABICYCLO-[4.1.0]-HEPTAN-2-ONE
![(1S,4S,6S)-1-METHYL-4-ISOPRENYL-7-AZABICYCLO-[4.1.0]-HEPTAN-2-ONE](/api/compound/Hae0etPXvaf.png?h=300&w=458 "(1S,4S,6S)-1-METHYL-4-ISOPRENYL-7-AZABICYCLO-[4.1.0]-HEPTAN-2-ONE")
Compound 10 (3R,5R)-5-ACETOXY-1-ETHYNYL-2-METHYL-3-[(4-NITROPHENYL)-CARBONYLOXY]-CYCLOHEX-1-ENE
![(3R,5R)-5-ACETOXY-1-ETHYNYL-2-METHYL-3-[(4-NITROPHENYL)-CARBONYLOXY]-CYCLOHEX-1-ENE](/api/compound/6KlNJL9URDH.png?h=300&w=458 "(3R,5R)-5-ACETOXY-1-ETHYNYL-2-METHYL-3-[(4-NITROPHENYL)-CARBONYLOXY]-CYCLOHEX-1-ENE")
Compound 11 (3R,5R)-5-ACETOXY-1-ETHYNYL-3-HYDROXY-2-METHYLCYCLOHEX-1-ENE
Compound 12 (3R,5R)-5-ACETOXY-3-(CHLOROACETOXY)-1-ETHYNYL-2-METHYLCYCLOHEX-1-ENE
Compound 13 (3R,5R)-5-ACETOXY-1-ETHYNYL-2-METHYL-3-PHTHALIMIDOCYCLOHEX-1-ENE
Compound 14 (3S,5R)-3-[(TERT.-BUTOXYCARBONYL)-AMINO]-1-ETHYNYL-5-HYDROXY-2-METHYLCYCLOHEX-1-ENE
![(3S,5R)-3-[(TERT.-BUTOXYCARBONYL)-AMINO]-1-ETHYNYL-5-HYDROXY-2-METHYLCYCLOHEX-1-ENE](/api/compound/AKr8ZWzsaBf.png?h=300&w=458 "(3S,5R)-3-[(TERT.-BUTOXYCARBONYL)-AMINO]-1-ETHYNYL-5-HYDROXY-2-METHYLCYCLOHEX-1-ENE")
Compound 15 (3S,5R)-3-[(TERT.-BUTOXYCARBONYL)-AMINO]-5-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYLCYCLOHEX-1-ENE
![(3S,5R)-3-[(TERT.-BUTOXYCARBONYL)-AMINO]-5-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYLCYCLOHEX-1-ENE](/api/compound/CwJ8QCEVqog.png?h=300&w=458 "(3S,5R)-3-[(TERT.-BUTOXYCARBONYL)-AMINO]-5-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYLCYCLOHEX-1-ENE")
Compound 16 (3S,5R)-5-ACETOXY-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYLCYCLOHEX-1-ENE
![(3S,5R)-5-ACETOXY-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYLCYCLOHEX-1-ENE](/api/compound/GZqE2sOi9UO.png?h=300&w=458 "(3S,5R)-5-ACETOXY-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYLCYCLOHEX-1-ENE")
Compound 17 (3S,5R)-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-5-HYDROXY-2-METHYLCYCLOHEX-1-ENE
![(3S,5R)-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-5-HYDROXY-2-METHYLCYCLOHEX-1-ENE](/api/compound/B8cb8uPJCsg.png?h=300&w=458 "(3S,5R)-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-5-HYDROXY-2-METHYLCYCLOHEX-1-ENE")
Compound 18 (3S,5S)-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYL-5-[(4-NITROPHENYL)-CARBONYLOXY]-CYCLOHEX-1-ENE
![(3S,5S)-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYL-5-[(4-NITROPHENYL)-CARBONYLOXY]-CYCLOHEX-1-ENE](/api/compound/FAHInHTNJHg.png?h=300&w=458 "(3S,5S)-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYL-5-[(4-NITROPHENYL)-CARBONYLOXY]-CYCLOHEX-1-ENE")
Compound 19 (3S,5S)-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-5-HYDROXY-2-METHYLCYCLOHEX-1-ENE
![(3S,5S)-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-5-HYDROXY-2-METHYLCYCLOHEX-1-ENE](/api/compound/B74AxD6TWZk.png?h=300&w=458 "(3S,5S)-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-5-HYDROXY-2-METHYLCYCLOHEX-1-ENE")
Compound 20 (3S,5R)-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYL-5-PHTHALIMIDOCYCLOHEX-1-ENE
![(3S,5R)-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYL-5-PHTHALIMIDOCYCLOHEX-1-ENE](/api/compound/KtTl5QtcMJ4.png?h=300&w=458 "(3S,5R)-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYL-5-PHTHALIMIDOCYCLOHEX-1-ENE")
Compound 21 (3S,5R)-5-[(TERT.-BUTOXYCARBONYL)-AMINO]-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYLCYCLOHEX-1-ENE
![(3S,5R)-5-[(TERT.-BUTOXYCARBONYL)-AMINO]-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYLCYCLOHEX-1-ENE](/api/compound/6OHEukn2Wr6.png?h=300&w=458 "(3S,5R)-5-[(TERT.-BUTOXYCARBONYL)-AMINO]-3-[(TERT.-BUTYLDIMETHYLSILYL)-OXY]-1-ETHYNYL-2-METHYLCYCLOHEX-1-ENE")
Compound 23 1-ALPHA-[(TERT.-BUTOXYCARBONYL)-AMINO]-25-HYDROXY-6,7-DEHYDROPREVITAMIN-D3
![1-ALPHA-[(TERT.-BUTOXYCARBONYL)-AMINO]-25-HYDROXY-6,7-DEHYDROPREVITAMIN-D3](/api/compound/HZ62UCkFTBf.png?h=300&w=458 "1-ALPHA-[(TERT.-BUTOXYCARBONYL)-AMINO]-25-HYDROXY-6,7-DEHYDROPREVITAMIN-D3")
Compound 24 3-BETA-[(TERT.-BUTOXYCARBONYL)-AMINO]-3-DEOXY-1-ALPHA,25-DIHYDROXY-6,7-DEHYDROPREVITAMIN-D3
![3-BETA-[(TERT.-BUTOXYCARBONYL)-AMINO]-3-DEOXY-1-ALPHA,25-DIHYDROXY-6,7-DEHYDROPREVITAMIN-D3](/api/compound/tsgpDHYK9T.png?h=300&w=458 "3-BETA-[(TERT.-BUTOXYCARBONYL)-AMINO]-3-DEOXY-1-ALPHA,25-DIHYDROXY-6,7-DEHYDROPREVITAMIN-D3")
Compound 27 1-ALPHA-[(TERT.-BUTOXYCARBONYL)-AMINO]-25-HYDROXYVITAMIN-D3
![1-ALPHA-[(TERT.-BUTOXYCARBONYL)-AMINO]-25-HYDROXYVITAMIN-D3](/api/compound/81ptIlJqwch.png?h=300&w=458 "1-ALPHA-[(TERT.-BUTOXYCARBONYL)-AMINO]-25-HYDROXYVITAMIN-D3")
Compound 28 3-BETA-[(TERT.-BUTOXYCARBONYL)-AMINO]-3-DEOXY-1-ALPHA,25-DIHYDROVITAMIN-D3
![3-BETA-[(TERT.-BUTOXYCARBONYL)-AMINO]-3-DEOXY-1-ALPHA,25-DIHYDROVITAMIN-D3](/api/compound/41Fun5OTzfm.png?h=300&w=458 "3-BETA-[(TERT.-BUTOXYCARBONYL)-AMINO]-3-DEOXY-1-ALPHA,25-DIHYDROVITAMIN-D3")
Citation
| Citation | J.ORG.CHEM.,68,1154(2003) |
|---|---|
| Journal | The Journal of Organic Chemistry |
| Issue | 3 |
| Volume | 68 |
| Page(s) | 1154-1157 |
| Year | 2002 |
| Author(s) | Daniel Oves, Miguel Ferrero, Susana Fernández, Vicente Gotor |
| Publisher | American Chemical Society (ACS) |
| DOI | 10.1021/jo026474t |