Spectra for:
Andrzej Wilk, Marcin K. Chmielewski, Andrzej Grajkowski, Lawrence R. Phillips, Serge L. Beaucage
Compound 1A 5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE
![5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE](/api/compound/zDr2QpDrO3.png?h=300&w=458 "5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE")
Compound 1B N(4)-BENZOYL-5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYCYTIDINE
![N(4)-BENZOYL-5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYCYTIDINE](/api/compound/GCQR21HKSiY.png?h=300&w=458 "N(4)-BENZOYL-5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYCYTIDINE")
Compound 1C N(6)-BENZOYL-5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYADENOSINE
![N(6)-BENZOYL-5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYADENOSINE](/api/compound/UL96SW9m7w.png?h=300&w=458 "N(6)-BENZOYL-5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYADENOSINE")
Compound 1D N(2)-ISOBUTYRYL-5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYGUANOSINE
![N(2)-ISOBUTYRYL-5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYGUANOSINE](/api/compound/JYIVfV8xUzC.png?h=300&w=458 "N(2)-ISOBUTYRYL-5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIISOPROPYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYGUANOSINE")
Compound 2 N-TERT.-BUTYL-4-HYDROXYBUTYRAMIDE
Compound 3 O-[3-[(N-TERT.-BUTYL)-CARBOXAMIDO]-1-PROPYL]-O,O-DIETHYL-PHOSPHATE
![O-[3-[(N-TERT.-BUTYL)-CARBOXAMIDO]-1-PROPYL]-O,O-DIETHYL-PHOSPHATE](/api/compound/LrlKkDHsTL.png?h=300&w=458 "O-[3-[(N-TERT.-BUTYL)-CARBOXAMIDO]-1-PROPYL]-O,O-DIETHYL-PHOSPHATE")
Compound 7 5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE
![5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE](/api/compound/CIBSNtSZgGA.png?h=300&w=458 "5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE")
Compound 8 5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-BUTYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE
![5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-BUTYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE](/api/compound/IuJgJQALakv.png?h=300&w=458 "5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-BUTYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE")
Compound 9 5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-ETHYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE
![5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-ETHYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE](/api/compound/KWakkjwSW29.png?h=300&w=458 "5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-ETHYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE")
Compound 10 5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-METHYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE
![5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-METHYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE](/api/compound/9ybCkQ1bbuD.png?h=300&w=458 "5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-TERT.-BUTYLCARBOXAMIDO)-METHYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE")
Compound 18 5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-METHYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE
![5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-METHYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE](/api/compound/7WBX1wpBHaa.png?h=300&w=458 "5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-METHYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE")
Compound 19 5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-ISOPROPYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE
![5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-ISOPROPYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE](/api/compound/6uLdnc49TBx.png?h=300&w=458 "5'-O-(4,4'-DIMETHOXYTRITYL)-3'-O-(N,N-DIETHYLAMINO)-[3-(N-ISOPROPYLCARBOXAMIDO)-1-PROPYLOXY]-PHOSPHINYL-2'-DEOXYTHYMIDINE")
Compound 22 O-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYL]-N,N,N',N'-TETRAISOPROPYLPHOSPHORDIAMIDITE
![O-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYL]-N,N,N',N'-TETRAISOPROPYLPHOSPHORDIAMIDITE](/api/compound/AbU6MK9RHBU.png?h=300&w=458 "O-[3-(N-TERT.-BUTYLCARBOXAMIDO)-1-PROPYL]-N,N,N',N'-TETRAISOPROPYLPHOSPHORDIAMIDITE")
2-(N-TERT.-BUTYLIMINO)-TETRAHYDROFURAN-HYDROBROMIDE
N-Isopropyl-4-hydroxybutyramide
N-tert-Butyl-3-hydroxypropionamide
N-TERT.-BUTYL-5-HYDROXYVALERAMIDE
N-TERT.-BUTYL-GLYCOLAMIDE
Citation
| Citation | J.ORG.CHEM.,67,6430(2002) |
|---|---|
| Journal | The Journal of Organic Chemistry |
| Issue | 18 |
| Volume | 67 |
| Page(s) | 6430-6438 |
| Year | 2002 |
| Author(s) | Andrzej Wilk, Marcin K. Chmielewski, Andrzej Grajkowski, Lawrence R. Phillips, Serge L. Beaucage |
| Publisher | American Chemical Society (ACS) |
| DOI | 10.1021/jo0258608 |