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Spectra for:
Yan Chen, John K. Snyder
Compound 1 2
TRICYCLO-[6.2.1.0-(3,9)]-UNDEC-5-EN-2-ONE
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Compound 5
EXO-2-TRICYCLO-[6.2.1.0-(3,9)]-UNDEC-5-ENYL-ACETATE
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Compound 6
EXO-4-TRICYCLO-[5.4.0.0-(3,7)]-UNDEC-9-ENYL-ACETATE
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Compound 7
EXO-TRICYCLO-[6.2.1.0-(3,9)]-UNDEC-5-EN-2-OL
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Compound 8
EXO-TRICYCLO-[6.2.1.0-(3,9)]-UNDECAN-2-OL
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Compound 9
TRICYCLO-[6.2.1.0-(3,9)]-UNDECAN-2-ONE
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Compound 10
3-OXA-TRICYCLO-[7.2.1.0-(4,10)]-DODECAN-2-ONE
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Compound 11
(1S*,2R*,7R*,9S*)-9-HYDROXYMETHYLBICYCLO-[5.3.0]-DECAN-2-OL
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Compound 13A
EXO-3,7-DIOXATETRACYCLO-[8.2.1.0-(4,11).0-(6,8)]-TRIDECAN-2-ONE
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Compound 13B
EXO-2,7-DIOXATETRACYCLO-[8.2.1.0-(4,11).0-(6,8)]-TRIDECAN-3-ONE
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Compound 13C
ENDO-3,7-DIOXATETRACYCLO-[8.2.1.0-(4,11).0-(6,8)]-TRIDECAN-2-ONE
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Compound 14
METHYL-(1S*,2R*,4R*,6S*,7S*,9S*)-2-HYDROXY-5-OXA-10-TRICYCLO-[6.3.0.0-(4,6)]-UNDECYL-METHANOATE
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Compound 15D
SYN-5-TERT.-BUTOXY-1-METHYLTETRACYCLO-[5.4.0.0-(2,4).0-(3,7)]-UNDECANE
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Compound 16D
(1R*,8R*,9S*,10R*)-10-TERT.-BUTOXY-8-METHYLTRICYCLO-[6.2.1.0-(3,9)]-UNDEC-2-ENE
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Compound 17B
TRICYCLO-[5.4.0.0-(3,7)]-UNDECAN-5-ONE
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Compound 17D
1-METHYLTRICYCLO-[5.4.0.0-(3,7)]-UNDECAN-5-ONE
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Compound 18D
(1R*,7R*,9S*,10R*)-10-TERT.-BUTOXY-7-METHYL-2-OXOBICYCLO-[5.3.0]-DECANE-9-CARBALDEHYDE
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Compound 20A
(1S*,2S*,3S*,4S*,5S*,6R*,7R*,9S*,10S*)-5-TERT.-BUTOXY-7,10-DIMETHYL-TETRACYCLO-[5.4.0.0-(2,4).0-(3,7)]-UNDECAN-9-OL
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Compound 20B
(1S*,2S*,3S*,4S*,5S*,6R*,7R*,9R*,10R*)-5-TERT.-BUTOXY-7,10-DIMETHYL-TETRACYCLO-[5.4.0.0-(2,4).0-(3,7)]-UNDECAN-9-OL
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Compound 21A
(1S*,2S*,3S*,4S*,5S*,6R*,7R*,9S*,10S*)-5-TERT.-BUTOXY-10-METHYL-TETRACYCLO-[5.4.0.0-(2,4).0-(3,7)]-UNDECAN-9-OL
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Compound 21B
(1R*,2S*,3S*,4S*,5S*,6R*,7S*,9R*,10R*)-5-TERT.-BUTOXY-10-METHYL-TETRACYCLO-[5.4.0.0-(2,4).0-(3,7)]-UNDECAN-9-OL
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Compound 21D
(1R*,2S*,3S*,4S*,5S*,6R*,7S*,9S*,10S*)-5-TERT.-BUTOXY-10-METHYL-TETRACYCLO-[5.4.0.0-(2,4).0-(3,7)]-UNDECAN-9-OL
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Compound 22
(1S*,2S*,3S*,4S*,5S*,6R*,7R*,9S*,10S*)-5-TERT.-BUTOXY-9-(TERT.-BUTYLDIMETHYLSILOXY)-7,10-DIMETHYLTETRACYCLO-[5.4.0.0-(2,4).0-(3,7)]-UNDECANE
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Compound 23
(1S*,2S*,3S*,4S*,5S*,6R*,7R*,9S*,10S*)-5-TERT.-BUTOXY-9-(TERT.-BUTYLDIMETHYLSILOXY)-10-METHYLTETRACYCLO-[5.4.0.0-(2,4).0-(3,7)]-UNDECANE
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Compound 24A
ENDO-5-TERT.-BUTOXYTETRACYCLO-[5.4.0.0-(2,4).0-(3,7)]-UNDECANE-9,10-DIOL
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Compound 24B
EXO-5-TERT.-BUTOXYTETRACYCLO-[5.4.0.0-(2,4).0-(3,7)]-UNDECANE-9,10-DIOL
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Compound 25A
(1R*,5S*,6S*,8S*,9S*,10R*)-10-TERT.-BUTOXY-5,8-DIMETHYLTRICYCLO-[6.2.1.0-(3,9)]-UNDEC-2-EN-6-OL
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Compound 25B
(1R*,5S*,6S*,8S*,9S*,10R*)-10-TERT.-BUTOXY-6-TERT.-BUTYLDIMETHYLSILOXY-5,8-DIMETHYLTRICYCLO-[6.2.1.0-(3,9)]-UNDEC-2-ENE
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Compound 26A
(1S*,3S*,6R*,7S*,9S*,10S*)-10-HYDROXY-1,9-DIMETHYLTRICYCLO-[5.4.0.0-(3,7)]-UNDECAN-5-ONE
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Compound 26B
(1S*,3S*,6R*,7S*,9S*,10S*)-10-TERT.-BUTYLDIMETHYLSILOXY-1,9-DIMETHYLTRICYCLO-[5.4.0.0-(3,7)]-UNDECAN-5-ONE
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Compound 27A
(1R*,5S*,6S*,8S*,9S*,10R*)-10-TERT.-BUTOXY-5-METHYLTRICYCLO-[6.2.1.0-(3,9)]-UNDEC-2-EN-6-OL
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Compound 27B
(1R*,5S*,6S*,8S*,9S*,10R*)-10-TERT.-BUTOXY-6-TERT.-BUTYLDIMETHYLSILOXY-5-METHYLTRICYCLO-[6.2.1.0-(3,9)]-UNDEC-2-ENE
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Compound 28A
(1S*,3S*,6R*,7S*,9S*,10S*)-10-HYDROXY-9-METHYLTRICYCLO-[5.4.0.0-(3,7)]-UNDECAN-5-ONE
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Compound 28B
(1S*,3S*,6R*,7S*,9S*,10S*)-10-TERT.-BUTYLDIMETHYLSILOXY-9-METHYLTRICYCLO-[5.4.0.0-(3,7)]-UNDECAN-5-ONE
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Compound 29A
ENDO-(1R*,5S*,6R*,8S*,9S*,10R*)-10-TERT.-BUTOXYTRICYCLO-[6.2.1.0-(3,9)]-UNDEC-2-ENE-5,6-DIOL
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Compound 29B
EXO-(1R*,5R*,6S*,8S*,9S*,10R*)-10-TERT.-BUTOXYTRICYCLO-[6.2.1.0-(3,9)]-UNDEC-2-ENE-5,6-DIOL
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Compound 30
(1S*,3S*,6R*,7S*,9R*,10S*)-9,10-DIHYDROXYTRICYCLO-[5.4.0.0-(3,7)]-UNDECAN-5-ONE
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Compound 31
(1R*,4S*,5S*,7S*,9S*,10R*)-10-TERT.-BUTOXY-5-TERT.-BUTYLDIMETHYLSILOXY-4-METHYL-2-OXO-BICYCLO-[5.3.0]-DECANE-9-CARBALDEHYDE
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Compound 32
(1S*,6S*,7S*,9S*,10R*,11R*)-11-TERT.-BUTOXY-7-TERT.-BUTYLDIMETHYLSILOXY-4-METHOXY-6-METHYL-2-OXATRICYCLO-[6.2.1.0-(3,9)]-DODECAN-2-OL
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Compound 33
(1R*,4S*,5S*,7S*,9S*,10R*)-10-TERT.-BUTOXY-5-TERT.-BUTYLDIMETHYLSILOXY-4-METHYL-9-(2,5-DIOXACYCLOPENTYL)-BICYCLO-[5.3.0]-DECAN-2-ONE
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Compound 34
METHYL-(1R*,4S*,5S*,7S*,9S*,10R*)-10-TERT.-BUTOXY-5-TERT.-BUTYLDIMETHYLSILOXY-4-METHYL-2-OXO-BICYCLO-[5.3.0]-DECANE-9-CARBOXYLATE
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Compound 35
(1R*,4S*,5S*,7S*,9S*,10R*)-10-TERT.-BUTOXY-5-TERT.-BUTYLDIMETHYLSILOXY-4,7-DIMETHYL-2-OXO-BICYCLO-[5.3.0]-DECANE-9-CARBALDEHYDE
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Compound 36A
(1R*,5S*,9R*,11S*,12S*,13R*)-13-TERT.-BUTOXY-7,7-DIMETHYL-6,8-DIOXATETRACYCLO-[9.2.1.0-(3,12).0-(5,9)]-TETRADEC-2-ENE
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Compound 36B
(1R*,5R*,9S*,11S*,12S*,13R*)-13-TERT.-BUTOXY-7,7-DIMETHYL-6,8-DIOXATETRACYCLO-[9.2.1.0-(3,12).0-(5,9)]-TETRADEC-2-ENE
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Compound 37A
(1R*,4S*,8R*,10S*,12S*,13R*)-13-TERT.-BUTOXY-6,6-DIMETHYL-2-OXO-5,7-DIOXATRICYCLO-[8.3.0.0-(4,8)]-TRIDECANE-12-CARBALDEHYDE
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Compound 37B
(1R*,4R*,8S*,10S*,12S*,13R*)-13-TERT.-BUTOXY-6,6-DIMETHYL-2-OXO-5,7-DIOXATRICYCLO-[8.3.0.0-(4,8)]-TRIDECYL-12-CARBALDEHYDE
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Citation
Citation
J.ORG.CHEM.,66,6943(2001)
Journal
The Journal of Organic Chemistry
Issue
21
Volume
66
Page(s)
6943-6957
Year
2001
Author(s)
Yan Chen, John K. Snyder
Publisher
American Chemical Society (ACS)
DOI
10.1021/jo010269g