Spectra for:
Haoyun An, Tingmin Wang, Martin A. Maier, Muthiah Manoharan, Bruce S. Ross, P. Dan Cook
Compound 1 3'-DEOXY-5'-O-(4,4'-DIMETHOXYTRITYL)-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-METHYL-5-METHYLURIDINE-TRIETHYLAMINE-SALT
![3'-DEOXY-5'-O-(4,4'-DIMETHOXYTRITYL)-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-METHYL-5-METHYLURIDINE-TRIETHYLAMINE-SALT](/api/compound/LELP9nvH8Qv.png?h=300&w=458 "3'-DEOXY-5'-O-(4,4'-DIMETHOXYTRITYL)-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-METHYL-5-METHYLURIDINE-TRIETHYLAMINE-SALT")
Compound 2 2',3'-DIDEOXY-5'-O-(4,4'-DIMETHOXYTRITYL)-2'-BETA-FLUORO-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-5-METHYLURIDINE-TRIETHYLAMINE-SALT
![2',3'-DIDEOXY-5'-O-(4,4'-DIMETHOXYTRITYL)-2'-BETA-FLUORO-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-5-METHYLURIDINE-TRIETHYLAMINE-SALT](/api/compound/KvsYQqQ1FV2.png?h=300&w=458 "2',3'-DIDEOXY-5'-O-(4,4'-DIMETHOXYTRITYL)-2'-BETA-FLUORO-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-5-METHYLURIDINE-TRIETHYLAMINE-SALT")
Compound 3 3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-5'-O-(4-METHOXYTRITYL)-2'-O-METHYL-5-METHYLURIDINE-TRIETHYLAMINE-SALT
![3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-5'-O-(4-METHOXYTRITYL)-2'-O-METHYL-5-METHYLURIDINE-TRIETHYLAMINE-SALT](/api/compound/BJY08TMQJqG.png?h=300&w=458 "3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-5'-O-(4-METHOXYTRITYL)-2'-O-METHYL-5-METHYLURIDINE-TRIETHYLAMINE-SALT")
Compound 3 2 3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-METHYL-5-METHYLURIDINE-TETRABUTYLAMMONIUM-SALT
![3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-METHYL-5-METHYLURIDINE-TETRABUTYLAMMONIUM-SALT](/api/compound/8UNodW13TMX.png?h=300&w=458 "3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-METHYL-5-METHYLURIDINE-TETRABUTYLAMMONIUM-SALT")
Compound 4 2',3'-Dideoxy-2'-beta-fluoro-3'-C-[(hydroxyphosphinyl)-methyl]-5'-o-(4-methoxytrityl)-5-methyluridine-triethylamine-salt
![2',3'-Dideoxy-2'-beta-fluoro-3'-C-[(hydroxyphosphinyl)-methyl]-5'-o-(4-methoxytrityl)-5-methyluridine-triethylamine-salt](/api/compound/5FEyoFMnTPf.png?h=300&w=458 "2',3'-Dideoxy-2'-beta-fluoro-3'-C-[(hydroxyphosphinyl)-methyl]-5'-o-(4-methoxytrityl)-5-methyluridine-triethylamine-salt")
Compound 5 3'-Deoxy-3'-C-[(hydroxyphosphinyl)]-methyl-5'-o-(4-methoxytrityl)-thymidine-triethylamine-salt
![3'-Deoxy-3'-C-[(hydroxyphosphinyl)]-methyl-5'-o-(4-methoxytrityl)-thymidine-triethylamine-salt](/api/compound/35Pn6J4PIwK.png?h=300&w=458 "3'-Deoxy-3'-C-[(hydroxyphosphinyl)]-methyl-5'-o-(4-methoxytrityl)-thymidine-triethylamine-salt")
Compound 6 3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-(2-METHOXYETHYL)-5'-O-(4-METHOXYTRITYL)-5-METHYLURIDINE-TRIETHYLAMINE-SALT
![3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-(2-METHOXYETHYL)-5'-O-(4-METHOXYTRITYL)-5-METHYLURIDINE-TRIETHYLAMINE-SALT](/api/compound/8CixuVcbFB8.png?h=300&w=458 "3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-(2-METHOXYETHYL)-5'-O-(4-METHOXYTRITYL)-5-METHYLURIDINE-TRIETHYLAMINE-SALT")
Compound 7 3'-Deoxy-3'-C-[(hydroxyphosphinyl)-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-4-N-(N-methylpyrrolidin-2-ylidene)-5-methylcytidine
![3'-Deoxy-3'-C-[(hydroxyphosphinyl)-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-4-N-(N-methylpyrrolidin-2-ylidene)-5-methylcytidine](/api/compound/96EzmJM0t97.png?h=300&w=458 "3'-Deoxy-3'-C-[(hydroxyphosphinyl)-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-4-N-(N-methylpyrrolidin-2-ylidene)-5-methylcytidine")
Compound 8 3'-Deoxy-3'-C-[[(2-cyanoethoxy)-(diisopropylamino)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-thymidine
![3'-Deoxy-3'-C-[[(2-cyanoethoxy)-(diisopropylamino)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-thymidine](/api/compound/41HKmOcotVX.png?h=300&w=458 "3'-Deoxy-3'-C-[[(2-cyanoethoxy)-(diisopropylamino)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-thymidine")
Compound 9 3'-Deoxy-3'-C-[[(2-cyanoethoxy)-(diisopropylamino)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-5-methyluridine
![3'-Deoxy-3'-C-[[(2-cyanoethoxy)-(diisopropylamino)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-5-methyluridine](/api/compound/Jv8ZuWB4E1H.png?h=300&w=458 "3'-Deoxy-3'-C-[[(2-cyanoethoxy)-(diisopropylamino)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-5-methyluridine")
Compound 15 5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-DEOXY-2'-O-METHYL-3'-C-(2-PHENYLETHENYL)-5-METHYLURIDINE
Compound 16 5'-O-(TERT.-BUTYLDIPHENYLSILYL)-2',3'-DIDEOXY-2'-BETA-FLUORO-3'-C-(2-PHENYLETHENYL)-5-METHYLURIDINE
Compound 18 5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-DEOXY-2'-O-(2-METHOXYETHYL)-3'-C-(2-PHENYLETHENYL)-5-METHYLURIDINE
Compound 19 5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-DEOXY-3'-C-(HYDROXYMETHYL)-2'-O-METHYL-5-METHYLURIDINE
Compound 20 5'-O-(TERT.-BUTYLDIPHENYLSILYL)-2',3'-DIDEOXY-2'-BETA-FLUORO-3'-C-(HYDROXYMETHYL)-5-METHYLURIDINE
Compound 22 5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-DEOXY-3'-C-(HYDROXYMETHYL)-2'-O-(2-METHOXYETHYL)-5-METHYLURIDINE
Compound 23 5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-DEOXY-3'-C-(IODOMETHYL)-2'-O-METHYL-5-METHYLURIDINE
Compound 25 5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-DEOXY-3'-C-(IODOMETHYL)-THYMIDINE
Compound 26 5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-DEOXY-3'-C-(IODOMETHYL)-2'-O-(2-METHOXYETHYL)-5-METHYLURIDINE
Compound 28 5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-METHYL-5-METHYLURIDINE
![5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-METHYL-5-METHYLURIDINE](/api/compound/3fGcewfudZA.png?h=300&w=458 "5'-O-(TERT.-BUTYLDIPHENYLSILYL)-3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-METHYL-5-METHYLURIDINE")
Compound 29 5'-o-(Tert.-butyldiphenylsilyl)-2',3'-dideoxy-2'-beta-fluoro-3'-C-[(hydroxyphosphinyl)-methyl]-5-methyluridine
![5'-o-(Tert.-butyldiphenylsilyl)-2',3'-dideoxy-2'-beta-fluoro-3'-C-[(hydroxyphosphinyl)-methyl]-5-methyluridine](/api/compound/7B02BWqZtcG.png?h=300&w=458 "5'-o-(Tert.-butyldiphenylsilyl)-2',3'-dideoxy-2'-beta-fluoro-3'-C-[(hydroxyphosphinyl)-methyl]-5-methyluridine")
Compound 32 3'-Deoxy-3'-C-[(hydroxyphosphinyl)-methyl]-2'-o-methylthymidine
![3'-Deoxy-3'-C-[(hydroxyphosphinyl)-methyl]-2'-o-methylthymidine](/api/compound/9YbcDIdVPj9.png?h=300&w=458 "3'-Deoxy-3'-C-[(hydroxyphosphinyl)-methyl]-2'-o-methylthymidine")
Compound 32 3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-METHYLTHYMIDINE;SALT-FREE
![3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-METHYLTHYMIDINE;SALT-FREE](/api/compound/F3E4Jf9LLuK.png?h=300&w=458 "3'-DEOXY-3'-C-[(HYDROXYPHOSPHINYL)-METHYL]-2'-O-METHYLTHYMIDINE;SALT-FREE")
Compound 33 3'-DEOXY-3'-C-(IODOMETHYL)-2'-O-METHYL-5-METHYLURIDINE
Compound 34 2',3'-DIDEOXY-2'-BETA-FLUORO-3'-C-(IODOMETHYL)-5-METHYLURIDINE
Compound 35 3'-DEOXY-3'-C-(IODOMETHYL)-THYMIDINE
Compound 36 3'-DEOXY-3'-C-(IODOMETHYL)-2'-O-(2-METHOXYETHYL)-5-METHYLURIDINE
Compound 37 3'-DEOXY-5'-O-(4,4'-DIMETHOXYTRITYL)-3'-C-(IODOMETHYL)-2'-O-METHYL-5-METHYLURIDINE
Compound 38 2',3'-DIDEOXY-5'-O-(4,4'-DIMETHOXYTRITYL)-2'-BETA-FLUORO-3'-C-(IODOMETHYL)-5-METHYLURIDINE
Compound 42 3'-DEOXY-3'-C-(IODOMETHYL)-5'-O-(4-METHOXYTRITYL)-2'-O-METHYL-5-METHYLURIDINE
Compound 43 2',3'-DIDEOXY-2'-BETA-FLUORO-3'-C-(IODOMETHYL)-5'-O-(4-METHOXYTRITYL)-5-METHYLURIDINE
Compound 44 3'-DEOXY-3'-C-(IODOMETHYL)-5'-O-(4-METHOXYTRITYL)-THYMIDINE
Compound 45 3'-DEOXY-3'-C-(IODOMETHYL)-2'-O-(2-METHOXYETHYL)-5'-O-(4-METHOXYTRITYL)-5-METHYLURIDINE
Compound 50 3'-Deoxy-3'-C-[[(2-cyanoethoxy)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-thymidine
![3'-Deoxy-3'-C-[[(2-cyanoethoxy)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-thymidine](/api/compound/8URCRwlzRhV.png?h=300&w=458 "3'-Deoxy-3'-C-[[(2-cyanoethoxy)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-thymidine")
Compound 51 3'-Deoxy-3'-C-[[(2-cyanoethoxy)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-5-methyluridine
![3'-Deoxy-3'-C-[[(2-cyanoethoxy)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-5-methyluridine](/api/compound/FvSsUf9aZiy.png?h=300&w=458 "3'-Deoxy-3'-C-[[(2-cyanoethoxy)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-5-methyluridine")
Compound 53 3'-DEOXY-3'-C-(IODOMETHYL)-5'-O-(4-METHOXYTRITYL)-2'-O-METHYL-5-METHYLCYTIDINE
Compound 54 3'-Deoxy-3'-C-[(hydroxyphosphinyl)]-methyl-5'-o-(4-methoxytrityl)-2'-o-methyl-5-methylcytidine-triethylamine-salt
![3'-Deoxy-3'-C-[(hydroxyphosphinyl)]-methyl-5'-o-(4-methoxytrityl)-2'-o-methyl-5-methylcytidine-triethylamine-salt](/api/compound/AC0cXrmpsvV.png?h=300&w=458 "3'-Deoxy-3'-C-[(hydroxyphosphinyl)]-methyl-5'-o-(4-methoxytrityl)-2'-o-methyl-5-methylcytidine-triethylamine-salt")
Compound 56 3'-Deoxy-3'-C-[[(2-cyanoethoxy)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-4-N-(N-methylpyrrolidin-2-ylidene)-5-methylcytidine
![3'-Deoxy-3'-C-[[(2-cyanoethoxy)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-4-N-(N-methylpyrrolidin-2-ylidene)-5-methylcytidine](/api/compound/KeuC9aJl1zV.png?h=300&w=458 "3'-Deoxy-3'-C-[[(2-cyanoethoxy)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-4-N-(N-methylpyrrolidin-2-ylidene)-5-methylcytidine")
#10;3'-Deoxy-3'-C-[[(2-cyanoethoxy)-(diisopropylamino)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-4-N-(N-methylpyrrolidin-2-ylene)-5-methylcytidine
![#10;3'-Deoxy-3'-C-[[(2-cyanoethoxy)-(diisopropylamino)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-4-N-(N-methylpyrrolidin-2-ylene)-5-methylcytidine](/api/compound/5DAJLnoerrP.png?h=300&w=458 "#10;3'-Deoxy-3'-C-[[(2-cyanoethoxy)-(diisopropylamino)-phosphinyl]-methyl]-5'-o-(4-methoxytrityl)-2'-o-methyl-4-N-(N-methylpyrrolidin-2-ylene)-5-methylcytidine")
Citation
| Citation | J.ORG.CHEM.,66,2789(2001) |
|---|---|
| Journal | The Journal of Organic Chemistry |
| Issue | 8 |
| Volume | 66 |
| Page(s) | 2789-2801 |
| Year | 2001 |
| Author(s) | Haoyun An, Tingmin Wang, Martin A. Maier, Muthiah Manoharan, Bruce S. Ross, P. Dan Cook |
| Publisher | American Chemical Society (ACS) |
| DOI | 10.1021/jo001699u |