Spectra for:
Michael E. Jung, Akemi Toyota
Compound 2 (2S,3S,5R)-3-(TERT.-BUTYLDIPHENYLSILANYLOXY)-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID
Compound 3 (2S,3S,5R)-3-HYDROXY-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-TERT.-BUTYLESTER
Compound 4A (2S,3S,5R)-4-DEUTERIO-3-HYDROXY-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-TERT.-BUTYLESTER
Compound 5A (2R,3S,5R)-4-DEUTERIO-3-HYDROXY-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-TERT.-BUTYLESTER
Compound 5B (2S,4S,5R)-3-HYDROXY-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-2-(PHENYLSELENYL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-TERT.-BUTYLESTER
Compound 5C (2R,3S,5R)-3-HYDROXY-2-ALLYL-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-TERT.-BUTYLESTER
Compound 5D (2S,3S,5R)-3-BENZENESULFONYLOXY-2-FLUORO-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-TERT.-BUTYLESTER
Compound 5E (2S,3S,5R)-2-FLUORO-3-HYDROXY-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-TERT.-BUTYLESTER
Compound 6B 1-[(2R,4S,5R)-4-HYDROXY-5-HYDROXYMETHYL-5-PHENYLSELENYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![1-[(2R,4S,5R)-4-HYDROXY-5-HYDROXYMETHYL-5-PHENYLSELENYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/BPRjxzG5u9U.png?h=300&w=458 "1-[(2R,4S,5R)-4-HYDROXY-5-HYDROXYMETHYL-5-PHENYLSELENYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
Compound 6C 1-[(2R,4S,5S)-4-HYDROXY-5-HYDROXYMETHYL-5-(2-PROPENYL)-TETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![1-[(2R,4S,5S)-4-HYDROXY-5-HYDROXYMETHYL-5-(2-PROPENYL)-TETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/LRlBCOJ09yR.png?h=300&w=458 "1-[(2R,4S,5S)-4-HYDROXY-5-HYDROXYMETHYL-5-(2-PROPENYL)-TETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
Compound 6D 1-[(2R,4S,5R)-5-FLUORO-4-HYDROXY-5-HYDROXYMETHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![1-[(2R,4S,5R)-5-FLUORO-4-HYDROXY-5-HYDROXYMETHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/GOdUXmrhLPA.png?h=300&w=458 "1-[(2R,4S,5R)-5-FLUORO-4-HYDROXY-5-HYDROXYMETHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
Compound 7B 1-[(4AR,6R,7AS)-2,2-DIMETHYL-4A-PHENYLSELENYLTETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![1-[(4AR,6R,7AS)-2,2-DIMETHYL-4A-PHENYLSELENYLTETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/DiDoIDmN5pn.png?h=300&w=458 "1-[(4AR,6R,7AS)-2,2-DIMETHYL-4A-PHENYLSELENYLTETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
Compound 7C 5-METHYL-1-[(4AS,6R,7AS)-2,2-DIMETHYL-4A-(2-PROPENYL)-TETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-1H-PYRIMIDINE-2,4-DIONE
![5-METHYL-1-[(4AS,6R,7AS)-2,2-DIMETHYL-4A-(2-PROPENYL)-TETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-1H-PYRIMIDINE-2,4-DIONE](/api/compound/6KnscCI8y1c.png?h=300&w=458 "5-METHYL-1-[(4AS,6R,7AS)-2,2-DIMETHYL-4A-(2-PROPENYL)-TETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-1H-PYRIMIDINE-2,4-DIONE")
Compound 8 (2R,4R,5R)-1-[5-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYLMETHYL]-4-HYDROXYTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![(2R,4R,5R)-1-[5-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYLMETHYL]-4-HYDROXYTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/IXG9xOm4iPU.png?h=300&w=458 "(2R,4R,5R)-1-[5-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYLMETHYL]-4-HYDROXYTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
Compound 9 (2S,3R,5R)-3-HYDROXY-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-METHYLESTER
Compound 10A (2S,3R,5R)-2-DEUTERIO-3-HYDROXY-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-METHYLESTER
Compound 10B (2R,3R,5R)-3-HYDROXY-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-2-(PHENYLSELENYL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-METHYLESTER
Compound 10C (2S,3R,5R)-3-HYDROXY-2-METHYL-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-METHYLESTER
Compound 10D (2S,3R,5R)-3-HYDROXY-2-(2-PROPENYL)-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-METHYLESTER
Compound 10E (2R,3R,5R)-3-BENZENESULFONYLOXY-2-FLUORO-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-METHYLESTER
Compound 10F (2R,3R,5R)-2-FLUORO-3-HYDROXY-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-METHYLESTER
Compound 11A (2R,3R,5R)-2-DEUTERIO-3-HYDROXY-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-METHYLESTER
Compound 12B 1-[(2R,4R,5S)-4-HYDROXY-5-HYDROXYMETHYL-5-PHENYLSELENYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![1-[(2R,4R,5S)-4-HYDROXY-5-HYDROXYMETHYL-5-PHENYLSELENYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/BfW7baPsZcc.png?h=300&w=458 "1-[(2R,4R,5S)-4-HYDROXY-5-HYDROXYMETHYL-5-PHENYLSELENYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
Compound 12C 1-[(2R,4R,5R)-4-HYDROXY-5-HYDROXYMETHYL-5-METHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![1-[(2R,4R,5R)-4-HYDROXY-5-HYDROXYMETHYL-5-METHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/6szzAk6bv1h.png?h=300&w=458 "1-[(2R,4R,5R)-4-HYDROXY-5-HYDROXYMETHYL-5-METHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
Compound 12D 1-[(2R,4R,5R)-4-HYDROXY-5-HYDROXYMETHYL-5-(2-PROPENYL)-TETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![1-[(2R,4R,5R)-4-HYDROXY-5-HYDROXYMETHYL-5-(2-PROPENYL)-TETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/A9Rr55nW7A7.png?h=300&w=458 "1-[(2R,4R,5R)-4-HYDROXY-5-HYDROXYMETHYL-5-(2-PROPENYL)-TETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
Compound 12E 1-[(2R,4R,5S)-5-FLUORO-4-HYDROXY-5-HYDROXYMETHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![1-[(2R,4R,5S)-5-FLUORO-4-HYDROXY-5-HYDROXYMETHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/LBEcSKaP5B5.png?h=300&w=458 "1-[(2R,4R,5S)-5-FLUORO-4-HYDROXY-5-HYDROXYMETHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
Compound 13B 1-[(4AS,6R,7AR)-2,2-DIMETHYL-4A-PHENYLSELENYLTETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![1-[(4AS,6R,7AR)-2,2-DIMETHYL-4A-PHENYLSELENYLTETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/H4MRE54635U.png?h=300&w=458 "1-[(4AS,6R,7AR)-2,2-DIMETHYL-4A-PHENYLSELENYLTETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
Compound 13C 5-METHYL-1-[(4AS,6R,7AR)-2,2,4A-TRIMETHYLTETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-1H-PYRIMIDINE-2,4-DIONE
![5-METHYL-1-[(4AS,6R,7AR)-2,2,4A-TRIMETHYLTETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-1H-PYRIMIDINE-2,4-DIONE](/api/compound/ClUnOZNQHJQ.png?h=300&w=458 "5-METHYL-1-[(4AS,6R,7AR)-2,2,4A-TRIMETHYLTETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-1H-PYRIMIDINE-2,4-DIONE")
Compound 13D 5-METHYL-1-[(4AR,6R,7AR)-2,2-DIMETHYL-4A-(2-PROPENYL)-TETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-1H-PYRIMIDINE-2,4-DIONE
![5-METHYL-1-[(4AR,6R,7AR)-2,2-DIMETHYL-4A-(2-PROPENYL)-TETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-1H-PYRIMIDINE-2,4-DIONE](/api/compound/9Q0KdtMeyRe.png?h=300&w=458 "5-METHYL-1-[(4AR,6R,7AR)-2,2-DIMETHYL-4A-(2-PROPENYL)-TETRAHYDROFURO-[3,2-D]-[1,3]-DIOXIN-6-YL]-1H-PYRIMIDINE-2,4-DIONE")
(1R,9R,10R)-10-[[(4-METHOXYPHENYL)-DIPHENYL]-METHOXYMETHYL]-4-METHYL-8,11-DIOXA-2,6-DIAZATRICYCLO-[7.2.1.0(2,7)]-DODECA-3,6-DIEN-5-ONE
![(1R,9R,10R)-10-[[(4-METHOXYPHENYL)-DIPHENYL]-METHOXYMETHYL]-4-METHYL-8,11-DIOXA-2,6-DIAZATRICYCLO-[7.2.1.0(2,7)]-DODECA-3,6-DIEN-5-ONE](/api/compound/EVWgvVbMHDC.png?h=300&w=458 "(1R,9R,10R)-10-[[(4-METHOXYPHENYL)-DIPHENYL]-METHOXYMETHYL]-4-METHYL-8,11-DIOXA-2,6-DIAZATRICYCLO-[7.2.1.0(2,7)]-DODECA-3,6-DIEN-5-ONE")
(2R,4R,5R)-1-[4-(TERT.-BUTYLDIPHENYLSILANYLOXY)-5-HYDROXYMETHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![(2R,4R,5R)-1-[4-(TERT.-BUTYLDIPHENYLSILANYLOXY)-5-HYDROXYMETHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/BlLJK2mw88X.png?h=300&w=458 "(2R,4R,5R)-1-[4-(TERT.-BUTYLDIPHENYLSILANYLOXY)-5-HYDROXYMETHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
(2R,4R,5R)-1-[5-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYL]-4-(TERT.-BUTYLDIPHENYLSILANYLOXY)-TETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![(2R,4R,5R)-1-[5-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYL]-4-(TERT.-BUTYLDIPHENYLSILANYLOXY)-TETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/BOgbVW7HdLF.png?h=300&w=458 "(2R,4R,5R)-1-[5-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYL]-4-(TERT.-BUTYLDIPHENYLSILANYLOXY)-TETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
(2S,3R,5R)-3-(TERT.-BUTYLDIPHENYLSILANYLOXY)-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID
(2S,3R,5R)-3-(TERT.-BUTYLDIPHENYLSILANYLOXY)-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-METHYLESTER
(2S,3S,5R)-3-(TERT.-BUTYLDIPHENYLSILANYLOXY)-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-2-CARBOXYLIC-ACID-TERT.-BUTYLESTER
1-[(2R,4S,5R)-4-(TERT.-BUTYLDIPHENYLSILANYLOXY)-5-HYDROXYMETHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![1-[(2R,4S,5R)-4-(TERT.-BUTYLDIPHENYLSILANYLOXY)-5-HYDROXYMETHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/6XhgvJ7s083.png?h=300&w=458 "1-[(2R,4S,5R)-4-(TERT.-BUTYLDIPHENYLSILANYLOXY)-5-HYDROXYMETHYLTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
1-[(2R,4S,5R)-5-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYL]-4-(TERT.-BUTYLDIPHENYLSILANYLOXY)-TETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![1-[(2R,4S,5R)-5-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYL]-4-(TERT.-BUTYLDIPHENYLSILANYLOXY)-TETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/BRbI9qhTVjP.png?h=300&w=458 "1-[(2R,4S,5R)-5-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYL]-4-(TERT.-BUTYLDIPHENYLSILANYLOXY)-TETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
1-[(2R,4S,5R)-5-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYL]-4-HYDROXYTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE
![1-[(2R,4S,5R)-5-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYL]-4-HYDROXYTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE](/api/compound/3BoE1HiClgp.png?h=300&w=458 "1-[(2R,4S,5R)-5-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYL]-4-HYDROXYTETRAHYDROFURAN-2-YL]-5-METHYL-1H-PYRIMIDINE-2,4-DIONE")
METHANESULFONIC-ACID-(2R,3S,5R)-2-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYL]-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-3-YL-ESTER
![METHANESULFONIC-ACID-(2R,3S,5R)-2-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYL]-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-3-YL-ESTER](/api/compound/IOHqo6UjLb1.png?h=300&w=458 "METHANESULFONIC-ACID-(2R,3S,5R)-2-[BIS-(4-METHOXYPHENYL)-PHENYLMETHOXYMETHYL]-5-(5-METHYL-2,4-DIOXO-3,4-DIHYDRO-2H-PYRIMIDIN-1-YL)-TETRAHYDROFURAN-3-YL-ESTER")
Citation
| Citation | J.ORG.CHEM.,66,2624(2001) |
|---|---|
| Journal | The Journal of Organic Chemistry |
| Issue | 8 |
| Volume | 66 |
| Page(s) | 2624-2635 |
| Year | 2001 |
| Author(s) | Michael E. Jung, Akemi Toyota |
| Publisher | American Chemical Society (ACS) |
| DOI | 10.1021/jo001223a |