| SpectraBase Spectrum ID |
3uHj0V3HUKm |
| Name |
Flunarizine |
| Source of Sample |
Biomol International, L.P. |
| Catalog Number |
Free base of CA-225 |
| Lot Number |
Free base of 3-P3063z |
| Accessory |
DurasamplIR II |
| CAS Registry Number |
52468-60-7 |
| Compound Type |
Pure |
| Copyright |
Copyright © 2012-2024 John Wiley & Sons, Inc. All Rights Reserved. |
| Formula |
C26H26F2N2 |
| InChI |
InChI=1S/C26H26F2N2/c27-24-12-8-22(9-13-24)26(23-10-14-25(28)15-11-23)30-19-17-29(18-20-30)16-4-7-21-5-2-1-3-6-21/h1-15,26H,16-20H2/b7-4+ |
| InChIKey |
SMANXXCATUTDDT-QPJJXVBHSA-N |
| Instrument Name |
Bio-Rad FTS |
| Sample Preparation Procedure |
The dihydrochloride salt was dissolved in 0.5 ml water in a test tube, and 1 drop of 30% NaOH solution was added, causing the clear solution to turn cloudy white. 1 ml dichloromethane was added to the test tube, which was shaken thoroughly using a vortex mixer. The test tube was spun in a centrifuge to separate the organic and aqueous layers. The bottom organic layer was retrieved with a pipette and placed in another clean test tube. Most of the solvent was evaporated from the tube using a flow of nitrogen gas, and the remaining solution was used to create a film on the diamond window for ATR-IR. |
| Source of Spectrum |
Forensic Spectral Research |
| Technique |
ATR-Film (MeCl2) (DuraSamplIR II) |
